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GC/MS analysis report for sample AD22493, September 2001

Machine-extracted title · confidence 95%

Laboratory results for sample AD22493 indicating other unknown compounds detected via GC/MS on September 27, 2001.

NYC-WTC_000086827–000086851

Folder label: “508 Scan 9/15/01 9/26/01

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Scanned page image, NYC-WTC_000086842
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2501\22493.D vial: 4 Acq On : 25 Sep 2001 5:22 pm Operator: 209 GALOS Sample : GC/MS unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Heneicosane Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T.

34.64 4.10 ug/1 483140 Chrysene-dl2 33.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 9L •^2 Docosane, 11-butyl- 366 C26H54 013475-76-8 91 3 Hexatriacontane 507 C36H74 000630-06-8 91 ^4 Eicosane, 7-hexyl-____________________ 366 C26H54 055333-99-8 91 Abundance Scan 3224 (34.642 min): 22493.D (-) m/z 56.95 100.00% 57

5000 85

1-r-p-r I I |113 141 34.40 34.60 34.80 35.00

■nZz-> 50 UU 100 a ,169 197 225 253 295 150 200 250 300 350 380 400 450 500 m/z 71.00 68.36% Abundance #42201: Heneicosane 57

85 5000 T-r-p-r 34.40 34.60 34.80 35.00 m/z 43.05 62.72% |113 j j /fy , . ........ 2^,296........... ' ' I ■n/z-> 50 100 150 200 250 300 350 400 450 500 <M3undance #73937; Docosane, ll-butyl- 57 V 34.40 34.60 34.80 35.00 5000- 85 m/z 85.05 47.92%

Ti/z-> 50 l.f.lVfV .. 300 100 ' 150 ' ' 2(^ ' ' 250 . ' ' 400 ' 450 ,366 ' ' 3^ 500 Abundance #59136: Hexatriacontane I 57 34.40 34.60 34.80 35.00 m/z 41.05 22.32% 5000 85

■nfe-> 50 1 100 150 200 239 250 ........ 379 407 435 300 350 400 450 478 506 500 A 34.40 34.60 34.80 35.00

22493.D NP091101.M Wed Sep 26 11:36:50 2001 Page 7

NYC-WTC_000086842

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NYC-WTC_000086842Source: NYC Law Department, mirrored locally

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