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GC/MS calibration table for TCLP analysis, Oct 2001

Machine-extracted title · confidence 95%

Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.

NYC-WTC_000086768–000086785

Folder label: “508 Scan

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\OCT0101\LBA.D Vial: 2 Acq On : 1 Oct 2001 2:41 pm Operator: 209 GALOS Sample : 9/14 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total 1 6.479 154 157 169 rVV2 22610 61116 1.10% 0.197% 2 7.755 293 296 306 rBV 45727 110322 1.98% 0.356% 3 11.648 715 720 729 rBV 42093 105741 1.90% 0.341% 4 11.785 729 735 751 rBV 1548795 3905790 70.22% 12.597% 5 15.402 1122 1129 1146 rBV 2423153 5363821 96.43% 17.299% 6 20.690 1698 1705 1726 rBV 2437858 5562138 100.00% 17.939% 7 25.124 2180 2188 2199 rBV2 2335922 5127502 92.19% 16.537% 8 29.540 2664 2669 2676 rBV 213312 390437 7.02% 1.259% 9 29.650 2676 2681 2689 rVB 37203 74516 1.34% 0.240% 10 30.733 2791 2799 2807 rBV 61905 117588 2.11% 0.379% 11 31.679 2895 2902 2907 rBV 157133 312759 5.62% 1.009% 12 31.771 2907 2912 2917 rW 116023 225543 4.05% 0.727% 13 32.762 3015 3020 3028 rVB 120747 231309 4.16% 0.746% 14 33.166 3056 3064 3076 rBV2 1856350 4547247 81.75% 14.665% 15 33.717 3117 3124 3134 rVB2 132819 292911 5.27% 0.945% 16 34.644 3220 3225 3233 rVB 102459 211162 3.80% 0.681% 17 35.535 3317 3322 3329 rBV 82776 178927 3.22% 0.577% 18 36.398 3411 3416 3424 rBV 50749 120164 2.16% 0.388% 19 37.288 3504 3513 3528 rBV2 1284569 4067618 73.13% 13.119%

Sum of corrected areas: 31006611 LBA.D NP091101.M Tue Oct 02 12:02:29 2001

NYC-WTC_000086772

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