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VOC analysis results, sample AE12737, June 2002

Machine-extracted title · confidence 95%

Laboratory report for volatile organic compounds in sample AE12737 analyzed on June 3, 2002.

NYC-WTC_000083807–000083872

Folder label: “524 6/3/02”

←Page 7 of 66→
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NYC 9/11 Public Portal Document niDrary bearcn compouna neporc

Data File C:\HPCHEM\l\DATA\02JUNE3\0603Bl.D Vial 2 Acq On 3 Jun 2002 10:31 am Operator 201-wb Sample lab blanlc Inst GC/MS Ins Mise Multiplr 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP052902.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 14.alpha.-Morphinan, 7,8-dideh Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T.

22.67 0.03 ug/L 25154 CHLOROBENZENE-D5 21.75

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 14.alpha.-Morphinan, 7,8-didehydro- 281 C19H23NO 017939-34-3 9 2 Morphinan, 7,8-didehydro-3-methoxy- 281 C19H23NO 001816-06-4 9 3 6,7-Benzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 5 4 1,2-Dihydroanthra[l,2-d]thiazole-2,281 C15H7NO3S 000000-00-0 5 Abundance Scan 1097 (22.672 min): 0603B1.D (-) m/z 281.00 100.00% 2!i1

WHW

22.40 22.60 22.80 23.00 44 Tp-n-T-p-rr-rp- m/z 282.10 28.52% •n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 A Abundance #39631:14.alpha.-Morphinan, 7,8-didehydro-3-methoxy-17-met 2$1 160

5000 22.40 22.60 22.80 23.00 44 m/z 283.10 18.75% 116 188 226 266 I I'''' I Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39628: Morphinan, 7,8-didehydro-3-methoxy-17-methyl-6-meth 2$1

22.40 22.60 22.80 23.00 m/z 43.90 6.87% 5000

44 160 188 226 266 I

Ti/z-> jL ........................ 40 ........ I... I,.,208,|l,,.......... 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39602: 6,7-Benzo-phenothiazine-5.5-dioxide 2$1 22.40 22.60 22.80 23.00

5000

217 232

-n/z--> 40 60 102118 A 264 II 80 100 120 140 160 180 200 220 240 260 280 q-rr-TT-p

0603B1.D HP052902.M Fri Jun 07 11:45:15 2002 Page 1

NYC-WTC_000083813

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NYC-WTC_000083813Source: NYC Law Department, mirrored locally

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