VOC analysis results, sample AE12531, May 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File C:\HPCHEM\l\DATA\02MAY24\0524C10C.D Vial 7 Acq On 25 May 2002 2:43 am Operator 201-wb Sample cal 10 Inst GC/MS Ins Mise Multiplr 1.00 MS Integration Params: GAS6.P Quant Time: Jun 3 11:31 2002 Quant Results File: HP051702.RES

Quant Method C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title VOCs BY EPA METHOD 524 Last Update Mon Jun 03 11:27:58 2002 Response via Initial Calibration DataAcq Meth HP051702

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-DIFLUOROBENZENE 15.12 114 1580268 5.00 ug/L 0.08 24) CHLOROBENZENE-D5 21.78 117 1534087 5.00 ug/L 0.07 52) 1,4-DICHLOROBENZENE-D4 26.95 152 756641 5.00 ug/L 0.07

System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.35 65 824216 5.34 ug/L 0.08 Spiked TUnount 5.000 Recovery = 106.80% 3) 4-BROMOFLUOROBENZENE 24.36 174 614486 5.51 ug/L 0.07 Spiked Amount 5.000 Recovery = 110.20% 25) TOLUENE-D8 18.47 98 1996818 4.77 ug/L 0.07 Spiked Amount 5.000 Recovery = 95.40%

Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.85 85 510005 8.59 ug/L 98 5) CHLOROMETHANE 5.37 50 1090529 11.52 ug/L 99 6) VINYL CHLORIDE 5.60 62 502264 10.52 ug/L 98 7) BROMOMETHANE 6.57 94 256303 10.19 ug/L 96 8) CHLOROETHANE 6.73 64 488126 10.33 ug/L 97 9) TRICHLOROFLUOROMETHANE 7.28 101 848168 9.59 ug/L 100 11) l,l,2-Trichloro-l,2,2-trif 8.17 101 461684 9.14 ug/L 99 • 12) ACETONE 8.26 43 501916 35.86 ug/L 98 13) 1,1-DICHLOROETHENE 8.62 61 1524803 13.42 ug/L 96 14) METHYLENE CHLORIDE 9.62 49 1437407 13.88 ug/L 95 15) METHYL TERT BUTYL ETHER 9.91 73 970386 12.09 ug/L 96 16) TRANS-1,2-DICHLOROETHENE 10.28 61 1577624 13.70 ug/L 89 17) 1,1-DICHLOROETHANE 11.17 63 1746441 14.00 ug/L 99 18) 2-BUT7\NONE (MEK) 12.00 43 599244 57.02 ug/L 92 19) 2,2-DICHLOROPROP7tNE 12.39 77 1022343 10.11 ug/L 99 20) CIS-1,2-DICHLOROETHENE 12.48 96 896025 13.24 ug/L 90 21) CHLOROFORM 12.82 83 1757658 13.17 ug/L 100 22) BROMOCHLOROMETHANE 13.20 49 797726 15.20 ug/L 84 23) 1,2-DICHLOROETHANE 14.54 62 1406127 14.10 ug/L 100 26) 1,1,1-TRICHLOROETHANE 13.72 97 1288781 10.33 ug/L 98 27) 1,1-DICHLOROPROPENE 14.05 75 1356567 11.68 ug/L 99 28) CARBON TETRACHLORIDE 14.30 117 1051884 10.25 ug/L 98 29) BENZENE 14.64 78 3205211 12.78 ug/L 100 30) TRICHLOROETHENE 15.92 95 973316 11.64 ug/L 95 31) 1,2-DICHLOROPROPANE 16.28 63 896115 13.24 ug/L 99 32) DIBROMOMETHANE 16.96 174 376479 11.48 ug/L 95 33) BROMODICHLOROMETHANE 16.79 83 1168864 11.87 ug/L 99 34) 2-CHLOROETHYL VINYL ETHER 17.28 63 231761 17.76 ug/L 99 35) METHYL ISO-BUTYL KETONE 17.35 58 479686 56.57 ug/L 86 36) CIS-1,3-DICHLOROPROPENE 17.89 75 1164225 12.22 ug/L 99 3 7) TOLUENE •18.64 91 3170266 12.38 ug/L 97 38) TRANS-1,3-DICHLOROPROPENE 18.92 75 840522 10.61 ug/L 98 39) 1,1,2-TRICHLOROETHANE 19.31 97 494626 12.54 ug/L 98 4 0) TETRACHLOROETHENE 20.09 166 834706 11.06 ug/L 93 41) 1,3-DICHLOROPROPANE 19.83 76 1019702 13.32 ug/L 99 42) DIBROMOCHLOROMETHANE 20.53 129 569321 11.94 ug/L 97 43) 1,2-DIBROMOETHANE 20.98 107 494530 12.04 ug/L 99 4 4) CHLOROBENZENE 21.86 112 1946287 12.55 ug/L 96 45) 1,1,1,2-TETRACHLOROETHANE 21.91 131 710091 11.86 ug/L 97 46) 2-HEXANONE 19.20 43 921269 56.77 ug/L 96 47) ETHYLBENZENE 21.89 91 3806407 12.62 ug/L 99 (#) = qualifier out of range (m) = manual integration 0524C10C.D HP051702.M Mon Jun 03 11:31:30 2002 Page 1

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