Volatile organic compound analysis results, sample AE07502, April 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File C:\HPCHEM\l\DATA\02APR03\0403C10C.D Vial 3 Acq On 4 Apr 2002 2:13 am Operator 201-wb Sample cal 10 Inst GC/MS Ins Mise Multiplr 1.00 MS Integration Params: RTEINT.P Quant Time: Apr 4 2:52 2002 Quant Results File: HP031802.RES

Quant Method : C:\HPCHEM\1\METHODS\HP031802.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Wed Apr 03 15:28:09 2002 Response via : Initial Calibration DataAcq Meth : HP031802

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1, 4-DIFLUOROBENZENE 15.08 114 2103369 5.00 ug/L 0.03 24) CHLOROBENZENE-D5 21.74 117 1885243 5.00 ug/L 0.03 52) 1,4-DICHLOROBENZENE-D4 26.92 152 953199 5.00 ug/L 0.03 System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.32 65 1049621 6.06 ug/L 0.03 Spiked Amount 5.000 Recovery = 121.20% 3) 4-BROMOFLUOROBENZENE 24.33 174 800008 4.71 ug/L 0.03 Spiked Amount 5.000 Recovery = 94.20% 25) TOLUENE-D8 18.44 98 2507350 5.49 ug/L 0.03 Spiked Amount 5.000 Recovery = 109.80% Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.85 85 1120388 16.12 ug/L 97 5) CHLOROMETHANE 5.45 50 986464 11.88 ug/L 100 6) VINYL CHLORIDE 5.57 62 783006 14.73 ug/L 97 7) BROMOMETHANE 6.56 94 703106 14.08 ug/L 98 8) CHLOROETHANE 6.69 64 660090 12.8'0 ug/L 100 9) TRICHLOROFLUOROMETHANE 7.26 101 1270371 12.12 ug/L 98 11) l,l,2-Trichloro-l,2,2-trif 8.16 101 16226 0.35 ug/L 98 12) ACETONE 8.22 43 443556 31.17 ug/L 99 13) 1,1-DICHLOROETHENE 8.58 61 1206462 9.60 ug/L 96 14) METHYLENE CHLORIDE 9.59 49 1080631 9.68 ug/L 96 15) METHYL TERT BUTYL ETHER 9.89 73 992827 8.80 ug/L 99 16) TRANS-1,2-DICHLOROETHENE 10.25 61 1237612 9.81 ug/L 92 17) 1,1-DICHLOROETHANE 11.15 63 1423302 9.84 ug/L 96 18) 2-BUTANONE (MEK) 11.97 43 512834 33.15 ug/L 97 19) 2,2-DICHLOROPROPANE 12.36 77 935705 8.33 ug/L 92 20) CIS-1,2-DICHLOROETHENE 12.46 96 815202 9.59 ug/L 98 21) CHLOROFORM 12.79 83 1635221 10.45 ug/L 99 22) BROMOCHLOROMETHANE 13.18 49 619574 9.54 ug/L 99 23) 1,2-DICHLOROETHANE 14.52 62 1177756 10.89 ug/L 99 26) 1,1,1-TRICHLOROETHANE 13.69 97 1269594 11.92 ug/L 97 27) 1,1-DICHLOROPROPENE 14.01 75 1097900 11.21 ug/L 96 28) CARBON TETRACHLORIDE 14.27 117 1109686 12.11 ug/L 98 29) BENZENE 14.61 78 2626860 10.77 ug/L 99 3 0) TRICHLOROETHENE 15.89 95 858026 11.26 ug/L 96 .31) 1,2 -DICHLOROPROPTU^E 16.24 63 656958 10.32 ug/L 98 32) DIBROMOMETHANE 16.91 174 396609 10.99 ug/L 92 33) BROMODICHLOROMETHANE 16.75 83 1107468 11.49 ug/L 99 34) 2-CHLOROETHYL VINYL ETHER 17.25 63 253535 9.98 ug/L 97 35) METHYL ISO-BUTYL KETONE 17.32 58 445338 40.96 ug/L 87 36) CIS-1,3-DICHLOROPROPENE 17.84 75 948895 10.28 ug/L 96 37) TOLUENE 18.61 91 2800965 10.72 ug/L 99. 38) TRANS-1,3-DICHLOROPROPENE 18.88 75 717268 10.53 ug/L 96 39) 1,1,2-TRICHLOROETHANE 19.27 97 442747 10.27 ug/L 97 40) TETRACHLOROETHENE 20.06 166 861434 11.14 ug/L 97 41) 1,3-DICHLOROPROPANE 19.80 76 839047 10.56 ug/L 97 42) DIBROMOCHLOROMETHTiNE 20.50 129 621595 11.16 ug/L 95 43) 1,2-DIBROMOETHANE 20.94 107 455619 10.36 ug/L 98 44) CHLOROBENZENE 21.83 112 1840647 10.46 ug/L 93 45) 1,1,1,2-TETRACHLOROETHANE 21.88 131 701934 11.30 ug/L 98 46) 2-HEXANONE 19.17 43 837989 41.64 ug/L 93 47) ETHYLBENZENE 21.86 91 3400200 11.19 ug/L 99 (#) = qualifier out' of range (m) = manual integration 0403C10C.D HP022702.M Thu Apr 04 08:32:52 2002 Page 1

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