VOC analysis results, sample AE11905, May 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File : C:\HPCHEM\l\DATA\02MAY22\0522C10C.D Vial 3 Acq On : 23 May 2002 5:59 am Operator 201-wb Sample : cal 10 Inst GC/MS Ins Mise : Multiplr 1.00 MS Integration Params: GAS6.P Quant Time: Jun 3 14:26 2002 Quant Results File: HP051702.RES Quant Method : C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Fri May 31 11:43:42 2002 Response via : Initial Calibration DataAcq Meth : HP052102

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-DIFLUOROBENZENE 15.07 114 1205032 5.00 ug/L 0.03 24) CHLOROBENZENE-D5 21.73 117 1042440 5.00 ug/L 0.02 52) 1,4-DICHLOROBENZENE-D4 26.90 152 536178 5.00 ug/L 0.02 System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.30 65 609905 5.18 ug/L 0.03 Spiked Amount 5.000 Recovery = 103.60% 3) 4-BROMOFLUOROBENZENE 24.31 174 443951 5.22 ug/L 0.02 Spiked Amount 5.000 Recovery = 104.40% 25) TOLUENE-D8 18.42 98 1510117 5.30 ug/L 0.02 Spiked Amount 5.000 Recovery = 106.00%

Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.83 85 315226 7.25 ug/L 98 5) CHLOROMETHANE 5.34 50 678075 9.40 ug/L 97 6) VINYL CHLORIDE 5.56 62 285317 7.67 ug/L 100 7) BROMOMETHTiNE 6.55 94 142089 7.73 ug/L 98 8) CHLOROETHT^E 6.68 64 327799 9.10 ug/L 97 9) TRICHLOROFLUOROMETHANE 7.25 101 580384 8.61 ug/L 100 11) l,l,2-Trichloro-l,2,2-trif 8.14 101 327803 8.51 ug/L 100 12) ACETONE 8.22 43 307492 28.81 ug/L 96 13) 1,1-DICHLOROETHENE 8.57 61 970832 11.21 ug/L 96 14) METHYLENE CHLORIDE 9.57 49 869638 11.01 ug/L 96 15) METHYL TERT BUTYL ETHER 9.88 73 630920 10.31 ug/L 97 16) TRANS-1,2-DICHLOROETHENE 10.23 61 999347 11.38 ug/L 90 17) 1,1-DICHLOROETHANE 11.14 63 1082158 11.38 ug/L 99 18) 2-BUTANONE (MEK) 11.97 43 355814 44.40 ug/L 94 19) 2,2-DICHLOROPROPANE 12.34 77 643722 8.34 ug/L 99 20) CIS-1,2-DICHLOROETHENE 12.45 96 587842 11.39 ug/L 98 21) CHLOROFORM 12.79 83 1130971 11.11 ug/L 98 22) BROMOCHLOROMETHANE 13.16 49 479699 11.99 ug/L 99 23) 1,2-DICHLOROETHANE 14.51 62 889876 11.70 ug/L 100 26) 1,1,1-TRICHLOROETHANE 13.67 97 876997 10.35 ug/L 99 27) 1,1-DICHLOROPROPENE 14.00 75 878065 11.12 ug/L 99 28) CARBON TETRACHLORIDE 14.27 117 730385 10.47 ug/L 99 29) BENZENE 14.61 78 1989095 11.67 ug/L 100 30) TRICHLOROETHENE 15.87 95 640017 11.27 ug/L 94 31) 1,2-DICHLOROPROPANE 16.23 63 560500 12.19 ug/L 97 3 2) DIBROMOMETHANE 16.91 174 252963 11.35 ug/L 99 33) BROMODICHLOROMETHANE 16.75 83 766695 11.46 ug/L 98 34) 2-CHLOROETHYL VINYL ETHER 17.23 63 152733 17.22 ug/L 99 35) METHYL ISO-BUTYL KETONE 17.32 . 58 298172 51.75 ug/L 91 36) CIS-1,3-DICHLOROPROPENE 17.84 75 741477 11.45 ug/L 99 37) TOLUENE 18.61 91 2035124 11.70 ug/L 99 38) TRANS-1,3-DICHLOROPROPENE 18.88 75 542229 10.06 ug/L 99 39) 1,1,2-TRICHLOROETHANE 19.26 97 298242 11.13 ug/L 99 4 0) TETRACHLOROETHENE 20.04 166 536835 10.47 ug/L 96 41) 1,3-DICHLOROPROPANE 19.80 76 589169 11.32 ug/L 98 42) DIBROMOCHLOROMETHANE 20.48 129 356542 11.00 ug/L 96 43) 1,2-DIBROMOETHANE 20.94 107 300393 10.77 ug/L 98 44) CHLOROBENZENE 21.81 112 1148327 10.90 ug/L 98 45) 1,1,1,2-TETRACHLOROETHANE 21.86 131 435496 10.70 ug/L 97 46) 2-HEXANONE 19.15 43 523112 47.43 ug/L 95 47) ETHYLBENZENE 21.86 91 2196555 10.72 ug/L 99 (#) =. qualifier out of range (m) = manual integration 0522C10C.D HP051702.M Mon Jun 03 14:26:27 2002 Page 1

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