VOC analysis results, sample AE11905, May 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File : C:\HPCHEM\l\DATA\02MAY22\0522C10A.D Vial: 3 Acq On : 22 May 2002 . 1:26 pm Operator: 201-wb Sample : cal 10 Inst ; GC/MS Ins Mise : Multiplr; 1.00 MS Integration- Params: GAS6.P Quant Time: Jun 3 14:16 2002 Quant Results File: HP051702.RES

Quant Method C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title VOCs BY EPA METHOD 524 Last Update Fri May 31 11:43:42 2002 Response via Initial Calibration DataAcq Meth HP052102

Internal- Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-DIFLUOROBENZENE 15.02 114 1159657 5.00 ug/L -0.02 24) CHLOROBENZENE-D5 21.69 117 1095081 5.00 ug/L -0.02 52) 1,4-DICHLOROBENZENE-D4 26.87. 152 549330 5.00 ug/L -0.02 System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.27 65 529858 4.68 ug/L 0.00 Spiked Amount 5.000 Recovery = 93.60% 3) 4-BROMOFLUOROBENZENE 24.28 174 439565 5.37 ug/L -0.02 Spiked Amount 5.000 Recovery = 107.40% 25) TOLUENE-D8 18.39 98 1405646 4.70 ug/L -0.02 Spiked Amount 5.000 Recovery = 94.00% Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.81 85 418007 9.42 ug/L 97 5) CHLOROMETHANE 5.33 50 660769 9.52 ug/L 97 6) VINYL CHLORIDE 5.55 62 356713 10.15 ug/L 99 7) BROMOMETHANE 6.52 94 177520 9.71 ug/L 100 8) CHLOROETH7V1E 6.66 64 345901 9.98 ug/L 98 9) TRICHLOROFLUOROMETHANE 7.21 101 597588 9.21 ug/L 100 11) 1,1,2-Trichloro-l, 2,2-trif 8.11 101 319323 8.61 ug/L 96 12) .ACETONE 8.19 43 266524 25.95 ug/L 99 13) 1,1-DICHLOROETHENE 8.53 61 730354 8.76 ug/L 99 14) METHYLENE CHLORIDE 9.54 49 711530 9.36 ug/L 98 ■ 15) METHYL TERT BUTYL ETHER 9.84 73 545423 9.26 ug/L 99 16) TRANS-1,2-DICHLOROETHENE 10.20 61 822572 9.73 ug/L 95 17) 1,1-DICHLOROETHANE 11.10 63 894818 9.78 ug/L 100 18) 2-BUTANONE (MEK) 11.92 43 318545 41.30 ug/L 96 19) 2,2-DICHLOROPROPANE 12.31 77 714499 9.62 ug/L 99 20) CIS-1,2-DICHLOROETHENE 12.40 96 497598 10.02 ug/L 96 21) CHLOROFORM 12.74 83 935959 9.56 ug/L 99 22) BROMOCHLOROMETHANE 13.11 49 396069 10.28 ug/L 95 23) 1,2-DICHLOROETHANE 14.46 62 724598 9.90 ug/L 98 26) 1,1,1-TRICHLOROETHANE 13.62 97 746404 8.38 ug/L 99 27) 1,1-DICHLOROPROPENE 13.94 75 750609 9.05 ug/L 98 28) CARBON TETRACHLORIDE 14.22 117 627441 8.56 ug/L 99 29) BENZENE 14.56 78 1669804 9.33 ug/L 99 30) TRICHLOROETHENE 15.83 95 538685 9.03 ug/L 99 31) 1,2-DICHLOROPROPANE 16.19 63 457582 9.47 ug/L 98 32) DIBROMOMETHANE 16.86 174 219791 9.39 ug/L 100 33) BROMODICHLOROMETHANE 16.70 83 644760 ■9.18 ug/L 100 ■34) 2-CHLOROETHYL VINYL ETHER 17.18 63 119206 12.80 ug/L 99 35) METHYL ISO-BUTYL KETONE 17.26 58 255117 42.15 ug/L 98 36) CIS-1,3-DICHLOROPROPENE 17.79 75 657657 9.67 ug/L 99 37) TOLUENE 18.56 91 1718387 9.40 ug/L 98 38) TRANS-1,3-DICHLOROPROPENE 18.83 75 478378 8.41 ug/L 100 39) 1,1,2-TRICHLOROETHANE 19.22 97 276991 9.84 ug/L 99 4 0) TETRACHLOROETHENE 20.01 166 516392 9.59 ug/L 98 41) 1,3-DICHLOROPROPANE 19.75 76 546696 10.00 ug/L 97 42) DIBROMOCHLOROMETHANE 20.45 129 336739 9.89 ug/L 95 43) 1,2-DIBROMOETHANE 20.89 107 286125 9.76 ug/L 99 44) CHLOROBENZENE 21.78 112 1090075 9.85 ug/L 99 45) 1,1,1,2-TETRACHLOROETHANE 21.83 131 415804 9.73 ug/L 97 46) 2-HEX.ANONE 19.12 43 485629 41.92 ug/L 100 47) ETHYLBENZENE 21.81 91 2079407 9.66 ug/L 100 (#) = qualifier out of range (m) = manual integration 0522C10A.D HP051702.M Mon Jun 03 14:16:42 2002 Page 1

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