VOC analysis results, sample AE10890, May 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File : C:\HPCHEM\l\DATA\02may07\0507R5.D Vial: 4 Acq On : 7 May 2002 1:58 pm Operator: 201-wb Sample : ref 5 Inst ; GC/MS Ins Mise : May 6, 2002 Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: May 7 14:37 2002 Quant Results File: HP042202.RES

Quant Method : C:\HPCHEM\1\METHODS\HP042202.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Mon May 06 11:52:45 2002 Response via : Initial Calibration DataAcq Meth : HP042202

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-DIFLUOROBENZENE 15.10 114 1493771 5.00 ug/L 0.02 24) CHLOROBENZENE-D5 21.78 117 1382490 5.00 ug/L 0.03 52) 1,4-DICHLOROBENZENE-D4 26.95 152 668301 5.00 ug/L 0.02

System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.34 65 645836 4.72 ug/L 0.02 Spiked Amount 5.000 Recovery = 94.40% 3) 4-BROMOFLUOROBENZENE 24.36 174 543717 4.92 ug/L 0.03 Spiked TVmount 5.000 Recovery = 98.40% 25) TOLUENE-D8 18.47 98 1777046 4.97 ug/L 0.03 Spiked Amount 5.000 Recovery = 99.40%

Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.87 85 369250 6.31 ug/L 99 5) CHLOROMETHANE 5.44 50 385053 5.12 ug/L 94 6) VINYL CHLORIDE 5.60 62 325581 6.70 ug/L 99 7) BROMOMETHANE 6.59 94 258560 6.60 ug/L 97 8) CHLOROETHANE 6.73 64 259912 6.10 ug/L 93 9) TRICHLOROFLUOROMETHANE 7.28 101 472926 6.41 ug/L 99 12) ACETONE 8.26 43 204052 16.06 ug/L 96 13) 1,1-DICHLOROETHENE 8.62 61 535956 4.33 ug/L 97 14) METHYLENE CHLORIDE 9.60 49 427951 3.66 ug/L 94 15) METHYL TERT BUTYL ETHER 9.91 73 278433 3.44 ug/L 96 16) TRANS-1,2-DICHLOROETHENE 10.28 61 504035 3.94 ug/L 91 17) 1,1-DICHLOROETHANE 11.17 63 562807 3.97 ug/L 97 18) 2-BUTANONE (MEK) 12.00 43 168423 13.63 ug/L 87 19) 2,2-DICHLOROPROPANE 12.38 77 427466 4.17 ug/L 99 20) CIS-1,2-DICHLOROETHENE 12.48 96 321304 4.54 ug/L 91 21) CHLOROFORM 12.82 83 600755 . 4.47 ug/L 98 22) BROMOCHLOROMETHANE 13.20 49 228059 3.68 ug/L 78 23) 1,2-DICHLOROETHANE 14.54 62 411520 3.98 ug/L 95 26) 1,1,1-TRICHLOROETHANE 13.71 97 . 476675 4.70 ug/L 98 27) 1,1-DICHLOROPROPENE 14.03 75 455070 4.32 ug/L 99 28) CARBON TETRACHLORIDE 14.30 117 415380 4.86 ug/L 97 29) BENZENE 14.64 78 1071684 4.42 ug/L 99 30) TRICHLOROETHENE 15.92 95 336899 4.33 ug/L 93 . 31) 1,2-DICHLOROPROPANE 16.28 63 255396 3.68 ug/L 97 32) DIBROMOMETHANE 16.94 174 129825 4.35 ug/L 98 33) BROMODICHLOROMETHANE 16.79 83 396513 4.45 ug/L 97 34) 2-CHLOROETHYL VINYL ETHER 17.26 63 310768 14.90 ug/L 97 35) METHYL ISO-BUTYL KETONE 17.35 58 138302 15.49 ug/L 89 36) CIS-1,3-DICHLOROPROPENE 17.88 75 341756 3.79 ug/L 98 37) TOLUENE 18.64 91 1104957 4.50 ug/L 99 38) TRANS-1,3-DICHLOROPROPENE 18.92 75 246798 3.91 ug/L 98 39) 1,1,2-TRICHLOROETHANE 19.31 97 157440 4.12 ug/L 95 40) TETRACHLOROETHENE 20.09 166 323248 4.78 ug/L 95 41) 1,3-DICHLOROPROPANE 19.84 76 298175 3.88 ug/L 97 42) DIBROMOCHLOROMETHANE 20.53 129 195481 4.44 ug/L 99 43).1,2-DIBROMOETHANE 20.98 107 150447 3.88 ug/L 97 44) CHLOROBENZENE 21.86 112 686316 4.64 ug/L 95 45) 1,1,1,2-TETRACHLOROETHANE 21.91 131 238040 4.43 ug/L 98 46) 2-HEXANONE 19.21 43 245387 14.41 ug/L 97 47) ETHYLBENZENE 21.90 91 1321569 4.74 ug/L 100 48) P & M-XYLENE 22.05 106 845212 9.31 ug/L 96

{#) = qualifier out of range (m) = manual integration 0507R5.D HP042202.M Tue May 07 14:37:23 2002 Page 1

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