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Volatile organic compound analysis results, sample AE08425, April 2002

Machine-extracted title · confidence 100%

Laboratory report listing volatile organic compounds and concentrations for sample AE08425 with method detection limit qualifiers.

NYC-WTC_000081817–000081915

Folder label: “524 4/9/02

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Scanned page image, NYC-WTC_000081822
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\l\DATA\02APR08\0408Bl.D Vial: 1 Acq On 8 Apr 2002 9:03 am Operator: 201-wb Sample lb Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\HP031802.M (RTE Integrator) Title VOCs BY EPA METHOD 524 Library C:\DATABASE\NBS75K.L ********************************************************************* Peale Number 1 Cyclotetrasiloxane, octamethyl Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

22.63 0.27 ug/L 213437 CHLOROBENZ ENE-D5 21.66

Hit# of 5 Tentative ID MW MolForm. CAS# Qual

1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 64 2 6,7-Benzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 9 3 3,6-Bis(N-dimethylamino)-9-ethylcar 281 C18H23N3 057103-04-5 9 4 Benzene, l-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 9 Abundance Scan 1096 (22.627 min): 0408B1 .D (-) m/z 281.25 100.00% 2f!1

5000

133 193007 249 265 22.40 22.60 22.80 23.00 45 59j? I ^7 I T I, I m/z 282.25 30.41% ' I'''' I' I' ' ' ' 1 ' ‘ ' I ' ‘ ' 1 I . I I . I . I I'' '' I ' ''' I ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 2$1

5000 22.40 22.60 22.80 23.00 m/z 283.35 15.90% 73 T. ■ ■ .163177/?^ T 235^^9 -rp-m-p- » ' ' I ’ • ' ' I ' ' ' ’I ' ' “' I ‘ ' 1 ' ' ' ' 1 ' ' ' ’ I ' ' ' Ti/Z“> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39602: 6,7-Benzo-phenothiazine-5,5-dioxide 2 (1

22.40 22.60 22.80 23.00 5000 m/z 193.15 11.35%

217 I 232 102 118 264 I ' I ''' '1' rpm-rp Tl/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39624:3,6-Bis(N-dimethylamino)-9-ethylcarbazole 2(1 22.40 22.60 22.80 23.00 m/z 133.15 11.27%

5000 266

141 208222236^1° I m/2-> 40 60 80 100 120 140 160 180 200 220 240 260 280 22.40 22.60 22.80 23.00

0408B1.D HP031802.M Mon Apr 15 12:39:18 2002 Page 1

NYC-WTC_000081822

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NYC-WTC_000081822Source: NYC Law Department, mirrored locally

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