GCMS analysis results for sample AD25377, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C;\HPCHEM\1\DATA\NOV1401\25376.D Vial: 11 Acq On : 15 Nov 2001 2:22 am Operator: 209 GALOS Sample ; gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

6.32 0.58 ug/1 94111 1,4-Dichlorobenzene-d4 11.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Hex^one 100 C6H12O 000589-38-8 74 2 Pentarie, 2,3,4-trimethyl- 114 C8H18 000565-75-3 40 3 Propanoic acid, 2-methyl-, 3-methyl 158 C9H18O2 002050-01-3 40 4 Tripecane 184 C13H28 000629-50-5 38 Abundance Scan 139 (6.319 min); 25376. D (-) m/z 43.05 100.00% 4(3 57

71 5000 100

6,00 6.20 6,40 6,60 1 ,,,,,,,, , .^,l| 51. ' I ' ' * ' I ' ■ I I ■ > I I ' 85 ■ I 1 m/z SYToy 88.95% nfe-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #63357; 3-Hexanone 43 57 29

5000 71 6.00 6.20 6.40 6.60 100 m/z 70.95 59.40% 85 A-' -'" 11 1-r-r-p I I ■ I ■ I 1 I ' I ' ’ ’ ' I ' tVz-> 20 30 40 50 60 70 80 90 100 110 120 Abundance 4)3 #64229; Pentane, 2,3,4-trimethyl- 71 M'/V, 6.00 6.20 6.40 6.60 5000 m/z 100.05 35.69%

27 55

I ^74 rI I I I 1 I ■ ' ■ ■ I I I ■ ■ I . 114 rTfe-> 20 30 40 50 60 70 80 90 100 110 120 fiJjundance #67439; Propanoic acid, 2-methyl-, 3-methylbutyl ester 43 6.00 6.20 6.40 6.60 71 “mTz 41.05 26708%

5000

55 I............. 101........................................... n/z-> ...... 20 30 I 40 50 60 70 80 90 100 110 120 6.00 6.20 6.40 6.60

25376.D NP103001.M Wed Nov 21 12:56:13 2001 Page 1

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