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GC/MS analysis results for sample AD23799, Nov 1 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23799 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089311–000089332

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089318
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3001\23799.D Vial: 10 Acq On : 30 Oct 2001 11:19 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 6.33 0.41 ug/1 108113 1,4-Dichlorobenzene-d4 11.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3 -Hexanojfe 100 C6H12O 000589-38-8 72 2 3-Pent^one, 2-methyl- 100 C6H12O 000565-69-5 59 : 3 Pentam5, 2,3,4-trimethyl- 114 C8H18 . 000565-75-3 43. 4 Pent^e, 3-bromo-________________ 150 C5HllBr 001809-10-5 38 Abundance / Scan 140 (6.326 min): 23799.D (-) m/z43.05 100.00% 43 7

71 553 100

AJ I . I . I . . I . , , , I . , . . I . , , . I 6.00 6.20 6.40 6.60 , , .... .^,11 ‘ I ' ' ' ' I m/z 57.00 96717% nfe-> 20 30 40 50 60 70 80 90 100 110 120

Ik,. . Abundance #1528: 3-Hexanone 43 57

29 71 5000 6.00 6.20 6.40 6.60 100 m/z 70.95 63.68% '■‘l ' ' I I Ti/k-> 20 30 40 50 60 70 80 90 100 110 120 &hi indannp #63398:3-Rentanone, 2-methyl-___ 5|7 43 T 6.00 6.20 6.40 6.60 5000 m/z 100.05 45.74% 100 71 85 ■nfe-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #64229; Pentane, 2,3.4-trimethyl- ^aog—Kgo-^^ ~m7z 41.05, 24.23%

5000

27 55 .. Il , |l| , , , . ...... ....■ 1H-; r^q-T-T-T-T-y-rT-T-T-q-T-TT-T^-TT-T-^ TlZZ-> 20 30 40 50 60 70 80 90 100 110 1^ > . 6.00 6.20 6.40 6.60

23799.D NP103001.M Thu Nov 01 13:16:35 2001 Page 1 ;

NYC-WTC_000089318

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NYC-WTC_000089318Source: NYC Law Department, mirrored locally

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