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GCMS analysis results for sample AD24880, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24880 conducted on November 19, 2001, noting unknown compounds.

NYC-WTC_000069040–000069050

Folder label: “GCMS Scan X 10/18/01 An 11/6/01

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Scanned page image, NYC-WTC_000069049
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NYC 9/11 Public Portal Document

Library Search Compound Report Data Pile : C:\HPCHEM\1\DATA\NOV0601\24880.D vial: 10 Acq On : 6 Nov 2001 9:34 pm Operator: 209 GALOS Sanple : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DAT2kBASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.58 0.55 ug/1 93857 1,4-Dichlorobenzene-d4 11.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-Dichloroh^zene-d4 003855-82-1 90 150 C6C12D4 2 Benzene-1,2/3,4-d4-, 5,6-dichloro- 002199-69-1 33 150 C6C12D4 3 2-Methyl-^^nitroaniline 000570-24-1 10 152 C7H8N2O2! 4 3,4-Methyienedioxyanisole_____________ 152 C8H8O3 000000-00-0 9 Abundance Scan 712 (11.578 min): 24880.D (-) Tm/z 149.90 100.00% 1ii0

5000

52 I 63 78 115

uJtX 100 110 120 130 140 150 160 m/z 151.90 T JX 11.20 11.40 11.60 11.80 12.00 71.25% TTfe-> 20 30 40 50 60 70 80 90 Abundance :#9593:1,4-Dichlorobenzene-d4 1ii0

5000 115 . I . . i I I I . I C| . < . . P' ■ ■ ■ I ■

78 1120 11.40 11.60 11.80 12.00 52 m/z 115.00 36747%

•nZz-> 20 30 35 40 50 JU 60 70 80 90 100 110 120 130 140 150 160 I ‘ ‘ ‘ ‘ I

Abundance #9592: Benzene-1.2,3,4-d4-, 5,6-dichloro- 1$0

115 11.20 11.40 11.60 11.80 12.00 5000 52 78 m/z 77.95 21.58%

35 87 I ‘ r ' '' I ‘' I'''' 1' ‘* 1 ‘ ‘ * P I I * * ' ’ I 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #66883:2-Methyl-6-nitroaniline ' 1 ‘ ‘ I ‘ ' 77 1!2 1120 11.40 11.60 11.80 12.00 m/z 52.00 14.31% 5000

1 106 52 94

TiZz-> 30

' 30 ' 40 ’ 1 • ’ ’ ’ 1 ’ 50 60 Jt 70 80 90 ■7 122 M(11 '■* I 100 110 120 130 140 150 160 T 11.20 11.40 11.60 11.80 12.00

24880.D NP103001.M Fri Nov 16 12:01:04 2001 Page 2

NYC-WTC_000069049

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NYC-WTC_000069049Source: NYC Law Department, mirrored locally

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