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GCMS analysis results for sample AD24491, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24491 conducted on November 13, 2001, identifying unknown compounds.

NYC-WTC_000068622–000068633

Folder label: “508 Scan X 10/16/01 A 11/5/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\NOV0501\24491.D Vial; 10 Acq On : 5 Nov 2001 8:45 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing ; OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge <100 prefer < Baseline drop else tangent > Peak separation; 5

Signal : TIC peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 6.332 ' 136 140 147 rBV 27011 58427 1.09% 0.211% 2 6.433 147 151 162 rW 42700 112892 2.10% 0.408% 3 6.681/ 174 178 187 rVB 28629 61217 1.14% 0.221% 4 7.700^ 286 289 303 rBV 69325 184504 3.43% 0.667% 5 11.574 ' 706 711 720 rBV 40972 97083 1.80% 0.351% 6 11.711^ 720 726 750 rW 1520229 3627364 67.38% 13.123% 7 15.319/ 1113 1119 1136 rBV 2318146 4931203 91.60% 17.839% 8 20.598^ 1687 1694 1707 rBV 2507395 5383672 100.00% 19.476% 9 25.023^ 2169 2176 2188 rBV2 2381298 5180382 96.22% 18.741% 10 33.065/ 3044 3052 3072 rBV2 1803709 4387030 81.49% 15.871%

11 37.159/ 3490 3498 3518 rBV2 1281743 3618508 67.21% 13.090%

Sum of corrected areas: 27642282 24491.D NP103001.M Fri Nov 09 12:27:21 2001

NYC-WTC_000068628

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NYC-WTC_000068628Source: NYC Law Department, mirrored locally

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