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GCMS analysis results for sample AD24873, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24873 identifying unknown compounds on November 19, 2001.

NYC-WTC_000068942–000068953

Folder label: “GCMS Scan X 10/17/01 An 11/6/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\NOV0601\24873.D Vial: 2 Acq On : 6 Nov 2001 1:46 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 6.330 136 140 147 rBV 28339 59953 1.01% 0.193% 2 6.431 147 151 162 rW 44680 117619 1.97% 0.379% 3 6.679 174 178 189 rVB 30173 71023 1.19% 0.229% 4 7.698 286 289 301 rBV 70386 190429 3.19% 0.613% 5 11.572 707 711 721 rBV2 47798 109688 1.84% 0.353%

6 11.710 721 726 743 rW 1679221 4033037 67.61% 12.982% 7 15.318 1113 1119 1137 rBV 2547352 5512704 92.41% 17.745% 8 20.596 1688 1694 1711 rBV 2754063 5965292 100.00% 19.202% 9 25.021 2169 2176 2189 rBV2 2703414 5800226 97.23% 18.671% 10 33.063 3044 3052 3067 rBV2 2137267 5058709 84.80% 16.284% 11 37.167 3490 3499 3519 rBV 1455970 4147125 69.52% 13.349%

Sum of corrected areas: 31065805 24873.D NP103001.M Fri Nov 16 11:52:21 2001

NYC-WTC_000068948

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NYC-WTC_000068948Source: NYC Law Department, mirrored locally

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