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GCMS analysis results for sample AD24487, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24487 conducted on November 13, 2001, identifying unknown compounds.

NYC-WTC_000068572–000068584

Folder label: “508 Scan X 10/16/01 A 11/5/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\NOV0501\24487.D Vial: 5 Acq On : 5 Nov 2001 3:51 pm Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise : Multiplr; 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title ; 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.309\ 134 138 145 rBV 25530 55247 1.13% 0.212% 2 6.419^ 146 150 161 rW 39610 113452 2.32% 0.436% 3 6.547\ 161 164 173 rW 21617 56400 1.15% 0.217% 4 6.667 X 173 177 188 rVB 28541 68375 1.40% 0.263% 5 7.6860 284 288 306 rBV 109697 300023 6.14% 1.152%

6 11.578x 706 712 721 rBV 35229 92237 1.89% 0.354% 7 11.707\ 721 726 743 rBV 1298083 3299485 67.52% 12.671% 8 15.324\ 1113 1120 1138 rBV 2011686 4449223 91.05% 17.087% 9 20.603\ 1688 1695 1712 rBV 2203612 4886492 100.00% 18.766% 10 25.027^ 2170 2177 2188 rBV2 2174235 4790763 98.04% 18.398%

11 33.060\ 3045 3052 3067 rBV2 1866631 4287234 87.74% 16.464% 12 37.164^ 3490 3499 3516 rBV2 1289400 3640392 74.50% 13.980%

Sum of corrected areas: 26039323 24487.D NP103001.M Fri Nov 09 12:00:30 2001

NYC-WTC_000068578

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NYC-WTC_000068578Source: NYC Law Department, mirrored locally

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