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GCMS analysis results for sample AD24489, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24489 conducted on November 13, 2001, identifying unknown compounds.

NYC-WTC_000068598–000068609

Folder label: “508 Scan X 10/16/01 A 11/5/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\NOV0501\24489.D Vial; 12 Acq On : 5 Nov 2001 10:42 pm Operator; 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling ; 1 Min Area: 1 % of largest Peak Start Thrs; 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation; 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.324- 135 139 144 rBV 29130 54783 1.00% 0.193% 2 6.425/ 147 150 161 rW 40632 111952 2.05% 0.394% 3 6.672 174 177 190 rVB 28303 67213 1.23% 0.237% 4 7.159Z/ 224 230 236 rBV 18434 58642 1.07% 0.206% 5 7.701/ 285 289 305 rBV 62047 160507 2.93% 0.565%

6 11.575 ' 706 711 720 rBV 42201 99232 1.81% 0.349% 7 11.712-/ 720 726 742 rBV 1505332 3672989 67.16% 12.931% 8 15.320 1113 1119 1137 rBV 2305580 4982957 91.11% 17.543% 9 20.599/1687 1694 1717 rBV 2531482 5469329 100.00% 19.256% 10 25.024/ 2169 2176 2189 rBV2 2443916 5336823 97.58% 18.789%

11 33.066/3044 3052 3071 rBV2 1879875 4612294 84.33% 16.238% 12 37.160/ 3490 3498 3519 rBV2 1355021 3776831 69.05% 13.297%

Sum of corrected areas: 28403552 24489.D NP103001.M Fri Nov 09 12:22:30 2001

NYC-WTC_000068604

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NYC-WTC_000068604Source: NYC Law Department, mirrored locally

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