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GCMS analysis results for sample AD24475, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24475 conducted on November 14, 2001, identifying unknown compounds.

NYC-WTC_000068474–000068484

Folder label: “GCMS Scan X 10/12/01 An 11/3/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\NOV0201\24475.D Vial: 19 Acq On 3 Nov 2001 8:32 am Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.58 0.52 ug/1 71597 1,4-Dichlorobenzene-d4 11.72

Hit# of 5 tentative ID MW MolForm CAS# Qual 1 1,4-Dichlc^obenzene-d4 150 C6C12D4 003855-82-1 90 2 Benzene-l/2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 50 3 3,4-Methylenedioxyanisole 152 C8H8O3 000000-00-0 9 4 3-AminoY4-methylbenzamide 150 C8H10N2O» _____ 019406-86-1 9 Abundance / Scan 712 (11.578 min): 24475.D (-) m/z 149.90 100.00% 1!i0

5000 115 52 78 38 44 11 20 11.40 11.60 11.80 12.00 62 Ti/z-> I. . I . ■ 11 I iVi I 11 30 40 50 .... I'll..,. m/z 151.90 60 70 80 90 100 110 120 130 140 150 160 67.23% Abundance #9593:1,4-Dichlorobenzene-d4 liiO

5CX)0 115 78 11,20 11.40 11,60 11,80 12.00 52 m/z 114.90 37.31%

Tlfe-> 30 35 40 ,,l....... Il„,s„ 100 50 60 70 80 90 41^ 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-. 5.6-dichloro- 1$0

115 11 20 11.40 11.60 11.80 12.00 5000 52 78 m/z 52.00 . 19.22%

35 .................. ■nfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #10146; 3,4-Methylenedioxyanisole 1$2 1120 11.40 11.60 11,80 12.00 137 m/z 78.05 16.75% 5000 79 107 51 .... fl.?.. I ' I ' ' ' ‘ I ' ' ' ' I ' ' ' ' I I ' I I I ' I ' ' I ' 121 T i •n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

24475.D NP103001.M Tue Nov 13 10:08:58 2001 Page 2

NYC-WTC_000068483

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NYC-WTC_000068483Source: NYC Law Department, mirrored locally

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