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GCMS analysis results for sample AD24220, Nov 6 2001

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Laboratory report documenting GCMS analysis of sample AD24220 conducted on November 6, 2001, noting unknown compounds.

NYC-WTC_000068055–000068069

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\NOV0101\24219.D Vial; 6 Acq On ; 1 Nov 2001 7;54 pm Operator; 209 GALOS Sample ; gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P Method ; C;\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title ; 209 625/TCLP calibration table Smoothing ; OFF Filtering; 5 Sampling ; 1 Min Area; 1 % of largest Peak Start Thrs; 0.2 Max Peaks; 100 Stop Thrs ; 0 Peak Location; TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation; 5

Signal ; TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.314 135 138 144 rBV 24337 50445 1.20% 0.228% 2 6.415 146 149 159 rW 35374 102505 2.45% 0.463% 3 6.553 160 164 168 rW 20668 48081 1.15% 0.217% 4 6.663 172 176 188 rVB 26880 64053 1.53% 0.289% 5 7.150 225 229 234 rBV 19325 57373 1.37% 0.259%

6 7.691 284 288 304 rBV 82886 250299 5.97% 1.130% 7 11.575 706 711 721 rBV 33302 82120 1.96% 0.371% 8 11.712 721 726 745 rW 1149264 2894968 69.08% 13.070% 9 15.320 1113 1119 1137 rBV 1888226 3980792 94.98% 17.972% 10 20.599 1687 1694 1721 rBV 1978353 4190974 100.00% 18.921% 11 25.024 2169 2176 2188 rBV 1806930 3909864 93.29% 17.652% 12 33.057 3043 3051 3070 rBV2 1537893 3474456 82.90% 15.686% 13 37.151 3489 3497 3512 rBV2 987706 2850055 68.00% 12.867% 14 39.639 3761 3768 3777 rVB6 13002 52639 1.26% 0.238% 15 41.594 3968 3981 3987 rBV4 16005 90506 2.16% 0.409% 16 44.046 4237 4248 4255 rBV7 8400 50943 1.22% 0.230%

Sum of corrected areas; 22150073 24219.D NP103001.M Tue Nov 06 11;49;48 2001

NYC-WTC_000068061

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NYC-WTC_000068061Source: NYC Law Department, mirrored locally

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