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GCMS analysis results, sample AD23994, Oct 2001

Machine-extracted title · confidence 100%

DEP lab report for GCMS analysis of sample AD23994 conducted on October 25, 2001, noting unknown compounds.

NYC-WTC_000067705–000067719

Folder label: “GCMS Scan X 10/4/01 An 10/18/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\OCT1701\23993.D Vial; 17 Acq On ; 18 Oct 2001 4;53 am Operator; 209 GALOS Sample ; gc/ms unknown Inst : GC/MS 209 Mise ; Multiplr: 1.00 MS Integration Params; LSCINT.P Method ; C;\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title ; 209 625/TCLP calibration table 7/16/01 Smoothing ; OFF Filtering; 5 Sampling ; 1 Min Area; 1 % of largest Peak Start Thrs; 0.2 Max Peaks; 100 Stop Thrs ; 0 Peak Location; TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation; 5 Signal ; TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.379 142 146 152 rBV 24214 47772 1.87% 0.348% 2 6.489 ’ 152 158 169 rW 39763 107281 4.21% 0.781% 3 6.617 169 172 180 rW 20013 46432 1.82% 0.338% 4 6.727 181 184 196 rVB 27008 62004 2.43% 0.451% 5 7.747 292 295 312 rBV 70540 177814 6.97% 1.295%

6 10.216 560 564 571 rVB 13421 28727 1.13% 0.209% 7 sl0.-^8 582 586 596 rBV 12215 28034 1.10% 0.204% 8 rbr621 712 717 727 rBV 22400 47557 1.87% 0.346% 9 11.758 727 732 747 rBV 776471 1852308 72.65% 13.486% 10 15.375 1119 1126 1143 rBV 1134362 2521484 98.90% 18.357%

11 20.654 1694 1701 1712 rBV 1171064 2549470 100.00% 18.561% 12 25.079 2176 2183 2195 rBV2 1100208 2386585 93.61% 17.375% 13 33.121 3051 3059 3076 rBV2 911420 2113752 82.91% 15.389% 14 37.234 3499 3507 3522 rBV2 627912 1766294 69.28% 12.859%

Sum of corrected areas; 13735514 23993.D NP101901.M Wed Oct 24 11;23:11 2001

NYC-WTC_000067711

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NYC-WTC_000067711Source: NYC Law Department, mirrored locally

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