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GCMS analysis results, sample AD25460, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD25460 conducted on November 26, 2001, noting unknown compounds.

NYC-WTC_000069644–000069658

Folder label: “GCMS Scan X 10/25/01 An 11/5/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\NOV1501\25460.D Vial; 4 Acq On ; 15 Nov 2001 7:13 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Method ; C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing ; OFF Filtering; 5 Sampling ; 1 Min Area: 1 % of largest Peak Start Thrs; 0.2 Max Peaks; 100 Stop Thrs : 0 Peak Location; TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 7.691 285 288 312 rBV 107847 334320 6.50% 1.189% 2 11.712 720 726 751 rBV 1338268 3536521 68.78% 12.582% 3 15.320 1113 1119 1133 rBV 2120007 4708515 91.58% 16.752% 4 20.599 1687 1694 1'701 rBV 2315077 5141525 100.00% 18.293% 5 25.014 2169 2175 2187 rBV2 2273335 5096696 99.13% 18.133% 6 25.161 2187 2191 2199 rVB 16665 56242 1.09% 0.200% 7 33.056 3044 3051 3067 rBV 1899824 4517315 87.86% 16.072% 8 36.747 3447 3453 3461 rBV2 26560 84883 1.65% 0.302% 9 37.160 3488 3498 3525 rBV2 1398767 4070164 79.16% 14.481% 10 38.060 3588 3596 3605 rBV3 31805 124984 2.43% 0.445% 11 39.629 3758 3767 3779 rBV2 30065 153661 2.99% 0.547% 12 41.576 3967 3979 3994 rBV5 26650 166853 3.25% 0.594% 13 44.018 4234 4245 4260 rBV5 15980 115543 2.25% 0.411%

Sum of corrected areas: 28107222 25460.D NP103001.M Wed Nov 21 12:42:39 2001

NYC-WTC_000069650

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NYC-WTC_000069650Source: NYC Law Department, mirrored locally

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