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GCMS analysis results for sample AD24218, Nov 6 2001

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Laboratory report documenting GCMS analysis of sample AD24218 conducted on November 6, 2001, noting unknown compounds.

NYC-WTC_000068022–000068036

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0101\24217.D Vial: 4 Acq On : 1 Nov 2001 5:57 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanol Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 6.66 0.42 ug/1 57577 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexan61 102 C6H14O 000626-93-7 83 2 2-Pent;anol, 4-methyl- 102 C6H14O 000108-11-2 74 3 2-Wtanol 116 C7H16O 000543-49-7 40 4 2-Bfeptanol, (S) -____________________ 116 C7H16O 006033-23-4 40 Abundant Scan 176 (6.663 min): 24217.D (-) m/z 44795 100.00% 4l5

5000

:iZz-> W>undance 6n 56 rrp^TTtkrr 69 .. 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 #63584:2-Hexanol 87 m/z 6.40 6.60 eTToO L 6.80 7.00 15.53%

45

5000 A ...... 6.40 6,60 6.80 7.00 69 ■m/z 41.05 13.69>% I tTTTJTTTTf+tTTpTTTJTTrlyTTTTpTTTJTTT+jTt-ITpTTTpT^^ nZz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63545:2-Pentanol. 4-methyl- 4|5 T 6.40 6.60 6,80 7.00 5000 m/z .43.00 12.42%

27 39 I 57 87 Ii'iIhiiiIIttp TJTTrlTTTTTpTTrpTTlyrlTTp-rTTpTT^^ Tife-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #64346:2-Heptanol T 4b 6.40 6.60 6.80 7.00 m/z 43.95 10.16% 5000

27 70 .‘•O'*

■nfe-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 ' 6.^ '7.60 '

24217.D NP103001.M Tue Nov 06 11:46:48 2001 Page 2

NYC-WTC_000068031

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NYC-WTC_000068031Source: NYC Law Department, mirrored locally

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