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GCMS analysis results for sample AD24218, Nov 6 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24218 conducted on November 6, 2001, noting unknown compounds.

NYC-WTC_000068022–000068036

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0101\24217.D Vial: 4 Acq On : 1 Nov 2001 5:57 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATMASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.42 0.71 ug/1 96270 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 'entative ID MW MolForm CAS# Qual 1 2-Hexanone 100 C6H12O 000591-78-6 90 2 Oxir , 2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 56 3 2-He: none, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 56 4 Methyl Isobutyl Ketone 100 C6H12O 000108-10-1 53 Scan 149 (6.415 min): 24217.D (-) m/z 427^5 100.00%! 4t3

58 5000

71 85 100 6.00' 's.^' 6.^' aeo' iso' ,,,,,,,,,,,,l Wz 57795 56.60% T)Zz-> a ' "30" ' 40 50 60 70 80 90 100 110 120 130 140 ^bundance #1556:2-Hexanone 413

58 —I........... .J . .0 , ______ J____ ' I ' ' 5000 6.00 6.20 6.40 6.^ 6.80 m/z SYTOO 20.70% 27 71 85 100 TiZz-> 20 f.... I ■ ab''' 40 ^60 I. , ,11,,, I, ,i,, I,,,, I,,.,,,,,, I.,,, I,,,, I, 70 80 90 100 110 120 130 140 Abundance #1530: Oxirane, 2-methyl-2-(1-methylethyl)- 43 58 6.bo' '5.26' ‘bm 'e.eo' 6.8q' 5000 ■m/z 41.05 14.48% 71

30 85 100 m/z-> 4' 20 " T" 30 "40I 80 ' dp' "ioo iib"i:a' w 50 O) 70 M>undance #11968:2-Hexanone, 4-hydroxy-3-propyl- 43 6.00 6.^' 6.^' 6.60 6.80 m/z 100.05 11.01% 58

11 50tX) 29

71 J I 85 100 .,1,, I ■, I , [, 11 ,,11.11,11,,, 140 ,A A

m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 6.00 6.20 6,40 6.60 6.80

24217.D NP103001.M Tue Nov 06 11:46:46 2001 Page 1

NYC-WTC_000068030

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NYC-WTC_000068030Source: NYC Law Department, mirrored locally

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