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GCMS calibration table for TCLP analysis, Nov 2 2001

Machine-extracted title · confidence 100%

Calibration data table for GCMS TCLP analysis listing surrogate compounds and response factors from November 2, 2001.

NYC-WTC_000067979–000067989

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File s C:\HPCHEM\1\DATA\OCT3101\LB.D Vial: 2 Acq On : 31 Oct 2001 5:05 pm Operator: 209 GALOS Saraple : 10/10 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Sraoothing : OFF Filtering: 5 Sampling ; 1 Min Area: 1 % of largest Peak Start Thrs; 0.2 - Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first raax last PK peak peak peak % of # rain scan scan scan TY height area % raax. total 1 6.318 135 139 146 rBV 31146 61303 1.28% 0.245% 2 6.419 147 150 162 rVV2 43413 130941 2.73% 0.522% 3 6.556 162 165 172 rW 25269 54343 1.13% 0.217% 4 6.666 174 177 187 rVB 31619 70079 1.46% 0.280% 5 7.695 285 289 307 rBV 78895 219745 4.57% 0.877% 6 11.569 705 711 721 rBV 36177 88614 1.84% 0.353% 7 11.706 721 726 743 rBV 1262812 3199753 66.59% 12.764% 8 15.314 1114 1119 1136 rBV 2021553 4450756 92.63% 17.754% 9 20.593 1688 1694 1715 rBV 2158604 4805020 100.00% 19.167% 10 25.018 2170 2176 2188 rBV2 2055544 4513812 93.94% 18.006% 11 29.186 2626 2630 2640 rBV 24269 65439 1.36% 0.261% 12 33.060 3044 3052 3065 rBV 1708896 3929440 81.78% 15.675% 13 37.154 3490 3498 3514 rBV2 1215041 3479523 72.41% 13.880%

Sura of corrected areas; 25068768 LB.D NP103001.M Fri Nov 02 17:17:13 2001

NYC-WTC_000067983

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NYC-WTC_000067983Source: NYC Law Department, mirrored locally

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GCMS sample extraction log table, Nov 2001 · Box DEP Box 60

NYC-WTC_000068400

Multi-page laboratory log table recording sample extraction details including volumes and drip rates for GCMS analysis in November 2001.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998

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