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GCMS analysis results for sample AD23995, Oct 29 2001

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Laboratory report documenting GCMS analysis of sample AD23995 conducted on October 29, 2001, noting unknown compounds.

NYC-WTC_000067752–000067766

Folder label: “GCMS Scan X 10/5/01 An 10/25/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\OCT2501\23995.D Vial: 3 Acq On : 25 Oct 2001 2:39 pm Operator: 209 GALOS San^le : gc/ms unknown Inst ! GC/MS 209 Mise Multiplr: 1,00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 6.337 138 141 148 rBV 41758 80337 1.69% 0.346% 2 6.438 148 152 163 rW 62748 157803 3.33% 0.679% 3 6.576 163 167 175 rVB 32294 65262 1.38% 0.281% 4 6.686 176 179 185 rVV2 38446 78393 1.65% 0.337% 5 7.714 287 291 307 rBV 109156 275347 5.80% 1.184% 6 11.597 709 714 723 rVB 34728 81751 1.72% 0.352% 7 11.735 723 729 745 rBV 1323534 3167831 66.76% 13.625% 8 15.343 1116 1122 1140 rBV 1987736 4431538 93.39% 19.060% 9 20.631 1691 1698 1711 rBV 2156337 4745416 100.00% 20.410% 10 25.065 2173 2181 2193 rBV2 2034273 4610770 97.16% 19.831% 11 33.098 3049 3056 3069 rBV2 1361620 3159560 66.58% 13.589% 12 37.201 3495 3503 3518 rBV2 842862 2396017 50.49% 10.305%

Sum of corrected areas: 23250025 23995.D NP101901.M Fri Oct 26 10:08:07 2001

NYC-WTC_000067758

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NYC-WTC_000067758Source: NYC Law Department, mirrored locally

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