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GCMS analysis results for sample AD23996, Oct 29 2001

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Laboratory report documenting GCMS analysis of sample AD23996 conducted on October 29, 2001, noting unknown compounds.

NYC-WTC_000067767–000067781

Folder label: “GCMS Scan X 10/5/01 An 10/25/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C;\HPCHEM\1\DATA\OCT2501\23996.D Vial: 4 Acq On : 25 Oct 2001 3:37 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 San^ling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 6.354 139 143 150 rBV 49709 101986 1.84% 0.384% 2 6.464 151 155 165 rW 80452 192597 3.48% 0.725% 3 6.593 165 169 176 rW 40638 86125 1.56% 0.324% 4 6.703 177 181 190 rVB 53817 114563 2.07% 0.431% 5 7.722 288 292 303 rBV 165821 366330 6.62% 1.379% 6 11.596 708 714 723 rBV 45195 99790 1.80% 0.376% 7 11.734 723 729 748 rBV 1627744 3799625 68.64% 14.300% 8 15.342 1115 1122 1141 rBV 2253080 5311734 95.95% 19.992% 9 20.630 1690 1698 1713 rBV 2412277 5535749 100.00% 20.835% 10 25.064 2173 2181 2194 rBV 2341504 5135320 92.77% 19.328% 11 33.097 3049 3056 3071 rBV2 1456965 3337686 60.29% 12.562% 12 37.209 3495 3504 3517 rBV2 855564 2488380 44.95% 9.365%

Sum of corrected areas: 26569885 23996.D NP101901.M Fri Oct 26 10:09:32 2001

NYC-WTC_000067773

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NYC-WTC_000067773Source: NYC Law Department, mirrored locally

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