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GCMS calibration table for TCLP analysis, Nov 2 2001

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Calibration data table for GCMS TCLP analysis listing surrogate compounds and response factors from November 2, 2001.

NYC-WTC_000067979–000067989

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data Pile s Cs\HPCHEM\l\DATA\OCT3101\LB.D Vials 2 Acq On s 31 Oct 2001 5s05 pm Operators 209 GALOS Sample s 10/10 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Times Nov 2 16s42 2001 Quant Results Files NP103001.RES Quant Method s Cs\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title s 209 625/TCLP calibration table Last Update s Fri Nov 02 16s41sl6 2001 Response via s Initial Calibration DataAcq Meth s NP101901

Compound R.T. Qlon Response Cone Unit Qvalue 23) 2-Nitrophenol 0.00 139 0 N.D. 24) 2,4-Dimethylphenol 0.00 107 0 N.D. 25) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 26) 2,4-Dichlorophenol 0.00 162 0 N.D. 27) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 2 8) Naphthalene 0.00 128 0 N.D. 29) Hexachlorobutadiene 0.00 225 0 N.D. 30) 4-Chloro-3-methylphenol 0.00 107 0 N.D. 34) Hexachlorocyclopentadiene 0.00 237 0 N.D. 35) 2,4,6-Trichlorophenol 0.00 196 0 N.D. 36) 2,4,5-Trichlorophenol 0.00 196 0 N.D. 37) 2-Chloronaphthalene 0.00 162 0 N.D. 38) Dimethylphthalate 19.97 163 587 N.D. 39) 2,6-Dinitrotoluene 0.00 165 0 N.D. 40) Acenaphthylene 0.00 152 0 N.D. 41) Acenaphthene 0.00 153 0 N.D. 42) 2,4-Dinitrophenol 0.00 184 0 N.D. 43) 4-Nitrophenol 21.22 65 345 N.D. 44) 2,4-Dinitrotoluene 0.00 165 0 N.D. 45) Diethylphthalate 22.10 149 13499 N.D. 46) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 47) Fluorene 0.00 166 0 N.D. 48) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 50) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 51) N-Nitrosodiphenylamine 0.00 168 0 N.D. 52) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 53) Hexachlorobenzene 0.00 284 0 N.D. 54) Pentachlorophenol 24.70 266 1647 N.D. 55) Phenanthrene 25.01 178 612 N.D. 56) Anthracene 25.01 178 612 N.D. 57) Di-n-butylphthalate 27.03 149 12282 N.D. 5 8) Fluoranthene 0.00 202 0 60) 3,3'-Dichlorobenzidine 0.00 252 0 z^Td. 61) Benzidine 29.19 184 38655 1.29 ug/ 97 63) Pyrene 0.00 202 0 64) Butylbenzylphthalate 0.00 149 0 N.D. 65) Benzo(a)anthracene 33.06 228 3132 N.D. 66) Bis(2-ethylhexyl)phthalate 33.33 149 4081 N.D. 67) Chrysene 33.13 228 526 N.D. 69) Di-n-Octylphthalate 35.06 149 205 N.D. 70) Benzo(b)fluoranthene 0.00 252 0 N.D.

(#) = qualifier out of range (m) = manual integration LB.D NP103001.M Pri Nov 02 16s46s43 2001 Page 2

NYC-WTC_000067980

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