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GCMS analysis results, sample AD23994, Oct 2001

Machine-extracted title · confidence 100%

DEP lab report for GCMS analysis of sample AD23994 conducted on October 25, 2001, noting unknown compounds.

NYC-WTC_000067705–000067719

Folder label: “GCMS Scan X 10/4/01 An 10/18/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1701\23993.D Vial: 17 Acq On : 18 Oct 2001 4:53 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplrz 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 1,4-Dichlorobenzene-d4 Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 11.62 0.51 ug/1 47557 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 Tentati ID MW MolForm CAS# Qual 1 1,4-Dichloroben^ne-d4 150 C6C12D4 003855-82-1 50 2 Benzene-1,2^^3<4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 33 3 4-Amino-2-;2nlorobenzonitrile 152 C7H5C1N2 020925-27-3 10 4 2-Methy3.z^-nitroani 1 ine 152 C7H8N2O2 000570-24-1 10 Abundance Scan 717 (11.621 min): 23993.D (-) m/z 149.90 100.00% 1!i0

5000 115 78 I I . . . J I . I tfVtI 1|YiI I I I I 52 ''38 ........ 111 f. 1 ■ ■ ■ 11.M 11.40 11.60 11.80 12.00 m/z 151.90 68.44% nfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 1$0

KX)0 115 I ' ' ' ' I ' ' 78 11.20 11.40 11.60 11.80 12.00 52 ■m72Tj;4;9^6 35.25% 35 I'' ■' I nfe-> 30 40 50 60 70 80 90 100 110 W 130 140 150 160 Abundance #9592: Benzene-1.2.3,4-d4-, 5,6-dichloro-

1 5 1!i0 ..... JV... 11.23 11.40 11.60 11.80 12.00 5000 52 78 "mTz 78.05 23.98%

87 Ti/z-> 35 I M40^m"^ 70 I I'''' I' 80 90 100 110 120 130 A T 140 150 160 Abundance #10110:4-Amino-2-chiorobenzonitrite 1$2 11.^ 11.40 11.60 11.80 1200 ■m/z 52.00 16.23%

5000

117 125 ? 76^ I I ‘' I Tlfe-> M "m" 70 M 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

23993.D NP101901.M Wed Oct 24 11:23:28 2001 Page 6

NYC-WTC_000067718

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NYC-WTC_000067718Source: NYC Law Department, mirrored locally

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