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GCMS analysis results, sample AD23993, Oct 2001

Machine-extracted title · confidence 100%

DEP lab report for GCMS analysis of sample AD23993 conducted on October 25, 2001, noting unknown compounds.

NYC-WTC_000067690–000067704

Folder label: “GCMS Scan X 10/4/01 An 10/18/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1701\23948.D Vial: 15 Acq On : 18 Oct 2001 2:58 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 6.63 0.47 ug/1 44927 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Hexanyl 102 C6H14O 000623-37-0 83 2 3-Pent2(nol 88 C5H12O 000584-02-1 40 3 3-Pe; anol, 2-methyl- 102 C6H14O 000565-67-3 38 4 d-R±l o-tetrofuranose, 4-c-cycloprop 200 C10H16O4 030571-50-7 36 Abundance Scan 173 (6.625 min): 23948.D(-) Hm/z 59.05 100.00% 5b

5000 73 43 6.20 6.40 6.60 6.80 7.00 4+ 54 m/z 54.95 78.83% .-I I

I Tife-> ' 'lb' " ' ’30' 40 50 60 70 80'' "sb" ' iob " iio Abundance #1762:3-HexanoI 5b

5000 31 43 73 4* 6.20 6.40 6.60 6.80 7.00 Wz 73.00 48.68%

n&-> '1'0' ' '20' ' '30 nI'I'. .| 4 102 40 50 60 70 80 90 100 110 Abundance #62943:3-PentanoI 5b 31 6.20 6.40 6.60 6.80 7.00 5000 m/z 42.95 28.80% 41

'' I'''' I ■' ‘ ‘ I I I ' ‘ ' I ' ' ' ' I ' ' ' ' 1 ' ‘ ‘ ' 1 ' ' ' ‘ I n/z->10 20 30 40 50 I60 70 80 90 100 110 Abundance #1781:3-PentanoI. 2-methyl- 6.^ 6.^ 6.^ 6.80 7.00 m/z41.0523.98% 5000 31 73

45 15 I I ' I ' ' ' ‘I ' ' ' ' I ' ' ‘ ' I ' ' ' ‘ I ' ' ' ' I ‘ I ' ' ' ' I ' ‘ ' 1 Tlfe-* 10 20 30 40 50 60 70 80 90 100 110 6.^' 6.^ 6.60 'e.So' '7.00

23948.D NP101901.M Wed Oct 24 11:22:00 2001 Page 3

NYC-WTC_000067700

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NYC-WTC_000067700Source: NYC Law Department, mirrored locally

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