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GCMS analysis results, sample AD23947, Oct 2001

Machine-extracted title · confidence 100%

DEP lab report for GCMS analysis of sample AD23947 conducted on October 25, 2001, noting unknown compounds.

NYC-WTC_000067651–000067674

Folder label: “GCMS Scan X 10/4/01 An 10/18/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT2301\23915.D Vial: 19 Acq On : 24 Oct 2001 5:24 am Operator; 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 3-Hexanol Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 6.58 0.56 ug/1 86614 1,4-Dichlorobenzene-d4 11.74 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 3-Hexanol 102 C6H14O 000623-37-0 90 2 2-Pentanol 2,3-dimethy1- 116 C7H16O 004911-70-0 53 3 2-Pentan( ' , 2,4-dimethyl- 116 C7H16O 000625-06-9 40 4 3-Pent ol 88 C5H12O 000584-02-1 40 ^bundance Scan 168 (6.583 min): 23915.D (-) in/z 59.00 100.00%

5000 73 43 Or/ I , , , , I , , , , I ,

6.20 6.40 6.60 6.80 7.00 107 135 i-t-rTyTTT-rp-rT*rj-TT-r-ijT-TT-ryT^^ in/z 55.00 79.62% Tift-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 ^burKbnce #63531:3-HexanoI 5P

5000 73 6.^ 6.^ RCT S,^ 7.00 43 m/z 7370^ 50.52% ft ■'1 'I'' 1' ' '10 " 2b" ' '30' 40 50 60 70 ' "ao "90 ''166' iio'w"w"w ^bundance #64357:2-Penlanol, 2.3^imethyk 5i9

6.^ 6.40 6.60 6.80 7.00 5000 m/z 27.60% 43 27 101 I I 83 tiA:-> ' 10 "do " 30' T 40 50 60 70 80 90 100 110 120 130 140 Mxindance #3370:2-Pentanol. 2,4-dimethyl- T-T-yT-T-r-T-y-r-TT-T-p-T-T-^^ 6.20 6.40 6.60 6.80 7.00 “m/z 41.05 21.52%

5000

15 1 ' I'''' I' 27 1 I 10 20 30 40 50 43

‘ ‘ I'''' I' d) 80 83 ____________ I______________ I___________________ ' I ’ ’ ’ ’ I ‘ 70 ’ I ‘' I' ' ' • I ’ ' ' • I ‘ ’ * 1 ’ ’ • ‘ 1 ‘ 90 101

100 110 120 130 140 jM 6.20 6.^ 6.OT 6.M 7.60

23915.D NP101901.M Thu Oct 25 12:11:57 2001 Page 4

NYC-WTC_000067665

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NYC-WTC_000067665Source: NYC Law Department, mirrored locally

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