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GCMS analysis results, sample AD23947, Oct 2001

Machine-extracted title · confidence 100%

DEP lab report for GCMS analysis of sample AD23947 conducted on October 25, 2001, noting unknown compounds.

NYC-WTC_000067651–000067674

Folder label: “GCMS Scan X 10/4/01 An 10/18/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File s C:\HPCHEM\1\DATA\OCT2301\23915.D Vial: 19 Acq On : 24 Oct 2001 5:24 am Operator: 209 GALOS San^le : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 3-Hexanone Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 6.34 0.48 ug/1 74570 1,4-Dichlorobenzene-d4 11.74 Hit# of 5 ■entative ID MW MolForm CAS# Qual 1 3-HexanoXe 100 C6H120 000589-38-8 90 2 3-Hexaj2one, 4-ethyl- 128 C8H16O 006137-12-8 59 3 3-Pentanone, 2-methyl- 100 C6H120 000565-69-5 49 4 ButXne, 2,2-dimethyl- 86 C6H14 000075-83-2 42 Abundance Scan 142 (6.344 min): 23915.D (-) m/z 43.05 100.00% 43 57 71 5000 100 ____ * 1 ‘ ‘ I • * ’ ' 1 ‘ * I 6.00 6.20 6.40 6.60 107 149 I tT-rpVH-p-r-r-r-[ I ' ‘ ' I ''1 * m/z 57700 88.23% Tife-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #1528:3-Hexanone 43 57

29 71 5000 6.00 6.^ " " geo " *' 100 m/z 71.00 64.32%

Hnrr+ ' I' ''I I ‘ ,, l....... I I'l H I I I I I i66"ii6”i»"i^"i46"i» uv nZz-> 20 30 40 50 60 70 80 90 Abundance #5043:3-Hexanone, 4-ethyl- 43 57 71 29 6.00 6.20 6.40 6.60 5000 m/z 100.05 33.65%

99 128 v|l|..... ’nk-> M M ' 40' ' 90 60 70 80 90 100 110 120 130 140 150 Abundance #63398:3-Pentanone, 2-methyl- ‘ ‘ 1 ‘ ‘ ‘ ‘ p ' ' I ' ' ' ' I ■ ‘ ‘ I 5l7 6.00 6.20 6.40 6.60 43 “m/z 41.05 25770% 5000 100 71

• I ‘‘' I'' ■' 11 I'' ■ I ■ ‘ I • I' I 85 ■ I • ‘ • I' ■ ‘ ■ 1' I ‘ ’ I nfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 6.00 6.20 6.40 6.60

23915.D NP101901.M Thu Oct 25 12:11:52 2001 Page 2

NYC-WTC_000067663

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NYC-WTC_000067663Source: NYC Law Department, mirrored locally

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