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GCMS analysis results, sample AD23903, Oct 2001

Machine-extracted title · confidence 100%

DEP lab report for GCMS analysis of sample AD23903 conducted on October 23, 2001, noting unknown compounds.

NYC-WTC_000067495–000067507

Folder label: “GCMS Scan X 10/2/01 An 10/17/01

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Scanned page image, NYC-WTC_000067506
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1701\23903.D Vial: 8 Acq On : 17 Oct 2001 8:09 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 . Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.62 0.49 ug/1 .... 50511 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-Dichlor«(nenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-X^,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 25 3 Benzaldehyde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 14 4 4-Ajzrno-2-chlorobenzonitrile _________ 152 C7H5C1N2i 020925-27-3 9 Abundance Scan 717 (11.620 tnin): 23903.D (-) Tm/z 149.90 100.00%! 1!0

5000 115 52 78 IILM 1140 1160 1180 1200 40 U-p-n-ti-rr ^**,■,^..,...1.1,. 87 m/z 151.90 58.35% nZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlofobenzene-d4 liiO

553 115 78 11.^ 11.40 11.60 11.80 12.00 52 m/z 114.90 . 37.03% 35 87 n&-> 30 '' 40' ' I ' ' ' ’ I ’ ' • ' 1 ' I ’ ’* ‘ J ' I ' • ' I 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2.3.4-d4-, 5.6-dichloro- liiO I " ■' I " n-' < ry-'i-T-r-r^-r-r 115 IIJp 11.40 11.60 11.80 12.00 5000 52 78 “m/z 77795 19797%

n/z-> 35 I T-p-rTTYT-rrTp^T-T-ryTT-TT-pr-r-t-t-j-T 30 40 50 X,... 1,1. .. 60 70 80 90 100 110 120 130 140 150 160 ,^14^ Abundance #66892: Benzaldehyde. 2-hydroxy-3-methoxy- f 152 11.^ 11,40 11.60 11,80 12.00 "m/z 52.00 16.03% 106 5000 53 81

’1*‘ ’I’'''I T 'I''‘’1»*I’I’ 92 122 136 T-p-n-r- nfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 1200

23903.D NP101901.M Tue Oct 23 12:49:47 2001 Page 4 NYC-WTC_000067506

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NYC-WTC_000067506Source: NYC Law Department, mirrored locally

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