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GCMS analysis results for sample AD23998, Oct 29 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD23998 conducted on October 29, 2001, noting unknown compounds.

NYC-WTC_000067796–000067810

Folder label: “GCMS Scan X 10/5/01 An 10/25/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT2501\23998.D Vial: 6 Acq On : 25 Oct 2001 5:35 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 1,4-Dichlorobenzene-d4 Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 11.59 0.52 ug/l 106858 1,4-Dichlorobenzene-d4 11.74 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-Dich^robenzene-d4 150 C6C12D4 003855-82-1 64 2 Benzen^l,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 38 3 Benzaldehyde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 10 4 4-Amipto-2-chlorobenzonitrile 152C7H5C1N2i 020925-27-3 9 ^bundance Scan 713 (11.590 min): 23998.D (-) m/z 149.90 100.00% Iio

5000 115

52 78 .................... .......................... 40 87 11.20 11.40 11,60 11.80 12.00 - m/z 151.90 64.84% •nfe-> Abundance 30 40 50 60 70 80 90 100 110 120 130 140 150 160 #^93:1,4-Dichlorobenzene-d4 (1 liiO

--rTT-rT-r-p-r-r-l-=fT-i4-r^-i-rTrTr^^ 5000 115 78 11.^ 11.40 11.60 11.80 12.00 52 m/z 115.00 41.16%

TiZz-> 30 35 40 .,1........il„,y„ 100 110 120 130 140 150.. 160 50 60 70 80 90 T

Abundance #9592: Benzene-1,2.3,4-<i4-, 5,6-dichloro-

115 1ii0 Jk 11.20 11.40 11.60 11.80 12.00 5000 52 78 m/z 777^5 22.23%

35 87 I I

a ' I ‘ ‘ I ' '' I ' ' ' ' I ' I ’ ' ' ' I ‘ ' I' -rp-TT-rj-r 'nfe-> 30 40 50 60 80 90 100 110 120 130 70 140 150 160 Abundance #66892: Benzaldehyde, 2-hydroxy-3-methoxy- 1!i2 1120 11.40 11,60 11.80 12.00 nTz 52.00 18.37% 106 5000 53 81

122 ’ ! ’ ' ’ ’ 1 ’ • ' ' I ' 92 "t+t ■7^ 136 JI’ ■ I ' ' ' ■ I ■ ■‘ ‘7 ■nfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 1.1.40 11.60 11.80 12.00

23998.D NP101901.M Fri Oct 26 10:12:27 2001 Page 6

NYC-WTC_000067809

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NYC-WTC_000067809Source: NYC Law Department, mirrored locally

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