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GCMS analysis report for sample AE07379, April 2002

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Laboratory report documenting GCMS analysis of sample AE07379 for unknown compounds conducted on April 25, 2002.

NYC-WTC_000061228–000061236

Folder label: “GCMS X 3/28/02 A 4/19/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

• Data File C:\MSDCHEM\l\DATA\041802\7379.D Vial: 28 Acq On 19 Apr 2002 7:47 am Operator: Bohllc Sample SAMPLE 7379 3/28/02, FB Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peale Number 1 Benzene-1,2,3,4-d4 -, 5,6-di... Concentration Ranlt 1

R.T. EstConc Area Relative to ISTD R.T.

10.26 1.00 ug/L 63867 1,4-Dichlorobenzene-d4 9.41

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzene-1,2,3,4-d4-, 5,6-dichlor... 150 C6D4C12 002199-69-1 86 2 1,4-Dichlorobenzene-d4 150 C6D4C12 003855-82-1 59 3 Dezaguanine $$ ICN 4221 $$ 3-Dea... 150 C6H6N4O 041729-52-6 47 4 1,2-Dichlorobenzene-d4 $$ Benzen... 150 C6D4C12 _____ 002199-69-1 38 Abundance Scan 1223 (10.265 min): 7379.D (-) m/z 150.00 100.00% 150

5000

52 115 .76 10.00 10.20 10.40 10.60 Ol II "' I" I' « i ' I • " ' I " " 1 I " p " ' I'' " I m/z 152.00 40.44% m/z-> 10 20_ 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #41699: Benzene-1,2,3,4-d4-, 5,6-dichloro- SS 1,2-Dichloro..'........ 150

115 5000 52 78 .............. 10.00 10.20 10.40 10.60 m/z 115.00 JoTtO^ 38 87

m/z-> 0 1^X4 ,1 ll, ' 99 124 'friWp I rfp , I l■|'|l 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 . . ............... I""

Abundance #41701: 1,4-Dichlorobenzene-d4 150

10.00 10.20 10,40 10,60 Sigil 115 m/z 52710 2^797%

52 78

40 12 2,® y 99 ,1 124 0 t-rp-r-TT I " " I ■n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130140150 160 Abundance #45713: Dezaguanine $$ ICN 4221 $$ 3-Deazaguanine $$ 4H-lm... 1$0 L rVi-r-j- 10.00 10.20 10.40 10.60 m/z 76.10 19.78%

w 5000 43 52 105 133 78 68 95 122 0 ■m-rp-r Tl/Z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 10.00 10.20 10.40 10.60

7379.D 5080402BBC.M Tue Apr 23 18:47:43 2002 Page 3

NYC-WTC_000061235

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NYC-WTC_000061235Source: NYC Law Department, mirrored locally

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