GCMS reference results for sample AE06800, April 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

. Data File C:\MSDCHEM\l\DATA\040502\REFF0405.D ■Vial: 40 Acq On 7 Apr 2002 3:51 am Operator: Bohlk Sample REF2 3/22/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Apr 08 05:47:38 2002 Quant Results File: 5080402.RES

Quant Method : C:\MSDCHEM\l\5973N\5080402.M (RTE Integrator) Title . : Quantitation For Method 508gcscan Last Update : Fri Apr 05 05:56:22 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.46 152 1133596 20.00 ug/L -0.01 10) Naphthalene-d8 12.94 136 4993025 20.00 ug/L 0.00 17) Acenaphthene-dlO 18.05 164 2912874 20.00 ug/L 0.00 29) Phenanthrene-dlO 22.41 188 4216780 20.00 ug/L -0.01 38) Chrysene-dl2 30.24 240 3273568 20.00 ug/L -0.01 44) Perylene-dl2 34.11 264 1997570 20.00 ug/L 0.00

System Monitoring Compounds 37) 2,4-DDD (SURR) 27.36 235 248328 5.93 ug/L 0.00 Spiked Amount 5.000 Recovery = 118.60%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 3.53 74 290361m 6.71 ug/L 3) bis(2-chloroethyl) ether 8.90 93 759793 12.06 ug/L 81 4) 1,3 - Dichlorobenze 9.29 146 465197 8.16 ug/L 99 5) 1,4 - Dichlorobenzene 9.51 146 492973 8.84 ug/L 99 6) 1,2 - Dichlorobenzene 9.88 146 446352 8.61 ug/L 92 .7) 2,2 ' - oxybis (1-Chloropr 10.34 45 1202311 12.36 ug/L 93 8) N-Nitroso-di-n-propylamine 10.67 70 530890 11.07 ug/L 94 9) Hexachloroethane 10.76 117 162828 7.61 ug/L 93 11) Nitrobenzene 11.01 77 687334 8.65 ug/L 97 12) Isophorone 11.73 82 1518527 10.58 ug/L 98 13) bis(2-Chloroethoxy) methan 12.47 93 944014 10.85 ug/L 97 14) 1,2,4-Trichlorobenzene 12.82 180 401128 9.28 ug/L 98 • 15) Naphthalene 12.99 128 1988681 11.54 ug/L 98 16) Hexachlorobutadiene 13.44 225 127700 5.97 ug/L 94 18) Hexachlorocyclopentadiene 15.52 237 18469 1.18 ug/L 90 19) 2-chloronaphthalene 16.42 162 978360 9.73 ug/L 98 20) Dimethylphthalate 17.52 163 1390620 11.88 ug/L 99 21) 2,6-Dinitrotoluene 17.62 165 245451 9.92 ug/L 97 ■ 22) Acenaphthylene 17.60 152 1488935 10.78 ug/L 98 23) Acenaphthene 18.14 153 1139531 11.66 ug/L 100 24) 2,4-Dinitrotoluene 18.77 165 276945 8.13 ug/L 99 25) Diethylphthalate 19.64 149 1350212 13.67 ug/L 98 26) 4-Chlorophenyl-phenyl ethe 19.81 204 575918 11:30 ug/L 98 27) Fluorene 19.67 166 1394166 12.52 ug/L 98 28) Azobenzen/ 1,2-Diphenylhyd 20.26 77 1927469 10.97 ug/L 95 30) N-Nitrosodiphenylamine 20.18 169 607921 8.21 ug/L 98 31) 4-Bromophenyl-phenyl ether 21.23 248 288920 11.46 ug/L 95 32) Hexachlorobenzene 21.26 284 278570 11.49 ug/L 80 33) Phenanthrene 22.47 178 1947359 12.52 ug/L 99 34) Anthracene 22.62 178 1718273 11.36 ug/L 99 35) Di-n-butylphthalate 24.57 149 2367568 13.45 ug/L 99 36) Fluoranthene 25.98 202 1966353 12.13 ug/L 85 39) Pyrene 26.60 202 2123040 11.10 ug/L 88 40) Butylbenzylphthalate 28.98 149 936138 11.29 ug/L 90 41) Benzo (a) antracene 30.21 228 1476565 11.26 ug/L 99 42) Bis (2-ethylhexyl) phthala 30.85 149 1334751 12.50 ug/L 98 43) Chrysene 30.30 228 1556170 12.39 ug/L 99 45) Di-n-Octylphthalate 32.70 149 1798154 9.39 ug/L 100 46) Benzo (b) fluoranthene 33.16 252 1187962 11.00 ug/L 93

(#) = qualifier out of range (m) = manual integration REFF0405.D 5080402.M Mon Apr 08 05:4'8:09 2002 Page 1

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