GCMS reference standard results for sample AE06049, April 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

. Data File C:\MSDCHEM\l\DATA\040502\REFB0405.D Vial: 6 Acq On 6 Apr 2002 12:32 am Operator: Bohlk Sample REF2 3/15/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Apr 08 05:40:29 2002 Quant Results File: 5080402.RES

Quant Method : C:\MSDCHEM\l\5973N\5080402.M (RTE Integrator) Title : Quantitation For Method 508gcscan Last Update : Fri Apr 05 05:56:22 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.47 152 1374252 20.00 ug/L 0.00 10) Naphthalene-d8 12.94 136 5923393 20.00 ug/L 0.00 17) Acenaphthene-dlO 18.06 164 3282359 20.00 ug/L 0.00 29) Phenanthrene-dlO 22.42 188 4680980 20.00 ug/L 0.00 38) Chrysene-dl2 30.24 240 3596152 20.00 ug/L 0.00 44) Perylene-dl2 34.12 264 1990086 20.00 ug/L 0.00

System Monitoring Compounds 37) 2,4-DDD (SURR) 27.36 235 205980 4.43 ug/L 0.00 Spiked Amount 5.000 Recovery = 88.60%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 3.54 74 244105m 4.66 ug/L 3) bis(2-chloroethyl) ether 8.90 93 577437 7.56 ug/L 82 4) 1,3 - Dichlorobenze 9.29 146 415860 6.02 ug/L 99 5) 1,4 - Dichlorobenzene 9.51 146 424136 6.28 ug/L 95 6) 1,2 - Dichlorobenzene 9.88 146 390785 6.22 ug/L 99 7) 2,2 ' - oxybis (1-Chloropr 10.35 45 1024517 8.69 ug/L 94 8) N-Nitroso-di-n-propylamine 10.67 70 479529 8.24 ug/L 94 9) Hexachloroethane 10.77 117 151759 5.85 ug/L 93 11) Nitrobenzene 11.02 77 555311 5.89 ug/L 97 12) Isophorone 11.73 82 1365114 8.02 ug/L 99 13) bis(2-Chloroethoxy) methan 12.47 93 799859 7.75 ug/L 98 14) 1,2,4-Trichlorobenzene 12.82 180 350923 6.85 ug/L 97 15) Naphthalene 12.99 128 1664283 8.14 ug/L 98 16) Hexachlorobutadiene 13.44 225 126123 4.97 ug/L 98 18) Hexachlorocyclopentadiene 15.52 237 18057 1.02 ug/L 94 19) 2-chloronaphthalene 16.42 162 781159 6.90 ug/L 99 20) Dimethylphthalate 17.52 163 1177528 8.93 ug/L 99 21) 2,6-Dinitrotoluene 17.62 165 202133 7.25 ug/L 98 22) Acenaphthylene 17.60 152 1250151 8.03 ug/L 99 23) Acenaphthene 18.14 153 952932 8.65 ug/L 97 24) 2,4-Dinitrotoluene 18.77 165 222104 5.79 ug/L 95 25) Diethylphthalate 19.65 149 1165973 10.48 ug/L 96 26) 4-Chlorophenyl-phenyl ethe 19.81 204 511029 8.90 ug/L 96 27) Fluorene 19.67 166 1192694 9.50 ug/L 98 28) Azobenzen/ 1,2-Diphenylhyd 20.26 77 1679892 8.48 ug/L 93 30) N-Nitrosodiphenylamine 20.18 169 616765 7.51 ug/L 98 31) 4-Bromophenyl-phenyl ether 21.23 248 245410 8.77 ug/L 91 32) Hexachlorobenzene 21.26 284 239306 8.89 ug/L 82 33) Phenanthrene 22.47 178 1694055 9.81 ug/L 99 34) Anthracene 22.62 178 1463869 8.72 ug/L 99 35) Di-n-butylphthalate 24.58 149 1965173 10.06 ug/L 98 36) Fluoranthene 25.98 202 1668421 9.27 ug/L 83 39) Pyrene 26.60 202 1827359 8.70 ug/L 85 40) Butylbenzylphthalate 28.98 149 738449 8.11 ug/L 90 41) Benzo (a) antracene 30.21 228 1243088 8.63 ug/L 99 42) Bis (2-ethylhexyl) phthala 30.85 149 1044871 8.91 ug/L 98 43) Chrysene 30.31 228 1362391 9.87 ug/L 98 45) Di-n-Octylphthalate 32.70 149 1290473 6.77, ug/L 99 46) Benzo (b) fluoranthene 33.16 252 902382 8.39 ug/L 90

(#) = qualifier out of range (m) = manual integration REFB0405.D 5080402.M Mon Apr 08 05:41:01 2002 Page 1

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