GCMS quantitative analysis results for sample AE06090, April 2002

NYC 9/11 Public Portal Document Quantitation Report (Not Reviewed)

Data File C:\MSDCHEM\l\DATA\04 04 02B\RFJ24 04.D Vial; 12 Acq On 5 Apr 2002 3:39 am Operator: Bohlk Sample REF2 3/1'5/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Apr 05 06:39:29 2002 Quant Results File: 5080402.RES

Quant Method : C:\MSDCHEM\l\5973N\5080402.M (RTE Integrator) Title : Quantitation For Method 508gcscan Last Update : Fri Apr 05 05:56:22 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1).1,4-Dichlorobenzene-d4 9.46 152 935426 20.00 ug/L -0.01 10) Naphthalene-d8 12.93 136 4028699 20.00 ug/L -0.01 17) Acenaphthene-dlO 18.05 164 2207391 20.00 ug/L 0.00 29) Phenanthrene-dlO 22.41 188 3162018 20.00 ug/L -0.01 38) Chrysene-dl2 30.23 240 2378847 20.00 ug/L -0.02 44) Perylene-dl2 34.11 264 1385710 20.00 ug/L -0.01

System Monitoring Compounds 37) 2,4-DDD (SURR) 27.35 ■ 235 209401 6.67 ug/L 0.00 Spiked Amount 5.000 Recovery = 133.40%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 3.53 74 159147 4.46 ug/L 87 3) bis(2-chloroethyl) ether 8.90 93 674413 12.97 ug/L 85 4) 1,3 - Dichlorobenze 9.30 ' 146 345078 7.34 ug/L 96 5) 1,4 - Dichlorobenzene . 9.50 146 376371 8.18 ug/L 99 6) 1,2 - Dichlorobenzene 9.88 146 346788 8.11 ug/L 98 7) 2,2 ' - oxybis (1-Chloropr 10.34 45 1105145 13.77 ug/L 94 8) N-Nitroso-di-n-propylamine 10.67 70 510083 12.88 ug/L 95 9) Hexachloroethane 10.77 117 91080 5.16 ug/L 90 11) Nitrobenzene 11.02 77 622682 9.71 ug/L 97 12) Isophorone 11.73 82 1402897 12.12 ug/L 96 13) bis(2-Chloroethoxy) methan 12.47 93 839798 11.96 ug/L 98 14) 1,2,4-Trichlorobenzene 12.82 180 319991 9.18 ug/L 97 15) Naphthalene 12.99 128 1709011 12.29 ug/L 99 16) Hexachlorobutadiene 13.45 225 55124 3.20 ug/L 93 18) Hexachlorocyclopentadiene 15.52 237 8446 0.71 ug/L 85 19) 2-chloronaphthalene 16.42 162 840892 11.04 ug/L 96 20) Dimethylphthalate 17.51 163 1169822 13.19 ug/L 98 21) 2,6-Dinitrotoluene 17.62 165 197145 10.51 ug/L 97 22) Acenaphthylene 17.60 152 1331555 12.72 ug/L 99 23) Acenaphthene 18.14 153 991445 13.38 ug/L 100 24) 2,4-Dinitrotoluene 18.77 165 222172 8.61 ug/L 91 25) Diethylphthalate 19.64 149 1126942 15.06 ug/L 99 26) 4-Chlorophenyl-phenyl ethe 19.81 204 474889 12.29 ug/L 97 27) Fluorene 19.67 166 1195938 14.17 ug/L 98 28) Azobenzen/ 1,2-Diphenylhyd 20.26 77 1663062 12.49 ug/L 93 30) N-Nitrosodiphenylamine 20.18 169 469334 8.46 ug/L 95 31) 4-Bromophenyl-phenyl ether 21.23 248 247530 13.10 ug/L 89 32) Hexachlorobenzene 21.26 284 223298 12.28 ug/L 79 33) Phenanthrene 22.47 178 1660855 14.24 ug/L 99 34) Anthracene 22.62 178 1459419 12.86 ug/L 98 35) Di-n-butylphthalate 24.57 149 1925110 14.58 ug/L 99 36) Fluoranthene 25.97 202 1632366 13.43 ug/L 84 3 9) Pyrene 26.61 202 1802892 12.97 ug/L 89 40) Butylbenzylphthalate 28.98 14 9 742751 12.33 ug/L 86 41) Benzo (a) antracene 30.21 228 1257582 13.20 ug/L 98 42) Bis (2-ethylhexyl) phthala 30: 85 149 1106110 14.26 ug/L 96 43) Chrysene 30.29 228 '1284602 14.07 ug/L 99 45) Di-n-Octylphthalate 32.70 149 1560418 11.75 ug/L 96 46) Benzo (b) fluoranthene 33.15 252 957510 12.78 ug/L 91

(#) = qualifier out of range (m) = manual integration RFJ2404.D 5080402.M Fri Apr 05 06:39:49 2002 Page 1

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