GCMS quantitative analysis results for sample AE06090, April 2002

NYC 9/11 Public Portal Document Quantitation Report (Not Reviewed)

Data File C:\MSDCHEM\1\DATA\ 04 04 O2B\RFJ14 04.D Vial: .11 Acq On 5 Apr 2002. 2:50 am Operator: Bohlk Sample REFl .3/15/02 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Apr 05 06:38:08 2002 Quant Results File: 5080402.RES

Quant Method : C:\MSDCHEM\l\5973N\5080402.M (RTE Integrator) Title : Quantitation For Method 508gcscan Last Update : Fri Apr 05 05:56:22 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.46 152 1137272 20.00 ug/L -0.01 10) Naphthalene-d8 12.94 136 5147752 20.00 ug/L 0.00 17) Acenaphthene-dlO 18.05 164 2917329 20.00 ug/L 0.00 29) Phenanthrene-dlO 22.42 188 4207548 20.00 ug/L 0.00 38) Chrysene-dl2 30.24 240 3355265 20.00 ug/L 0.00 44) Perylene-dl2 34.12, 264 2141814 20.00 ug/L 0.00

System Monitoring Compounds 37) 2,4-DDD (SURR) 27.35 235 227719 5.45 ug/L 0.00 Spiked Amount 5.000 . Recovery = 109.00%

.Target Compounds Qvalue 2) N-nitroso-dimethyl amine 3.52 74 210946 4.86 ug/L 89 3) bis(2-chloroethyl) ether 8.90 93 709362 11.22 ug/L 82 4) 1,3 - Dichlorobenze 9.29 146 340382 5.95 ug/L ' 99 5) 1,4 - Dichlorobenzene 9.50 146 380370 6.80 ug/L 99 6) 1,2 - Dichlorobenzene 9.88 146 358755 6.90 ug/L 100 7) .2,2 ' - oxybis (1-Chloropr 10.35 45 1160800 11.89 ug/L 94 8) N-Nitroso-di-n-propylamine 10.67 70 577803 12.00 ug/L 90 9) Hexachloroethane 10.77 117 99324 4.62 ug/L 93 11) Nitrobenzene 11.02 77 656161 8.01 ug/L 95 12) Isophorone 11.73 82 1566875 10.59 ug/L 97 13) bis(2-Chloroethoxy) methan 12.47 93 933442 10.41 ug/L 99 14) 1,2,4-Trichlorobenzene 12.82 180 323935 7.27 ug/L 99 15) Naphthalene 12.99 128 1767509 9.95 ug/L 100 16) Hexachlorobutadiene ■ 13.44 225 64113 2.91 ug/L 91 18) Hexachlorocyclopentadiene 15.52 237 9548 0.61 ug/L 89 19) 2-chloronaphthalene 16.42 162 .. 838575 8.33 ug/L 99 20) Dimethylphthalate 17.52 163 1306500 11.14 ug/L 100 21) 2,6-Dinitrotoluene 17.62 165 221568 8.94 ug/L 98 22) Acenaphthylene 17.60 152 1437785 10.40 ug/L 98 23) Acenaphthene 18.14 153 1038025 10.60 ug/L 99 24) 2,4-Dinitrotoluene 18.77 165 258853 7.59 ug/L 99 25) Diethylphthalate 19.64 149 1244757 12.58 ug/L 99 26). 4-Chlorophenyl-phenyl ethe 19.81 204 530365 10.39 ug/L 98 27) Fluorene 19.67 166 1291345 11.58 ug/L 99 28) Azobenzen/ 1,2-Diphenylhyd 20.26 77 1858366 10.56 ug/L 93 30) N-Nitrosodiphenylamine 20.18 169 710291 9.62 ug/L 98 31) 4-Bromophenyl-phenyl ether 21.23 248 259866 10.33 ug/L 88 •32) Hexachlorobenzene 21.26 284 228236 9.43 ug/L 83 33) Phenanthrene 22.47 178 1796263 11.58 ug/L 99 34) Anthracene 22.62 178 1594463 10.56 ug/L 99 35) Di-n-butylphthalate 24.57 149 2148360 12.23 ug/L 100 36) Fluoranthene 25.98 202 1821062. 11.26 ug/L 83 39) Pyrene 26.61 202 1973583 10.07 ug/L 84 40) Butylbenzylphthalate 28.98 149 829385 9.76 ug/L 83 41) Benzo (a) antracene 30.20 228 1417267 10.55 ug/L 100 42) Bis (2-ethylhexyl) phthala 30.85 149 1220778 11.16 ug/L 99 43) Chrysene 30.30 228 1465469 11.38 ug/L 98 45) Di-n-Octylphthalate 32.70 149 1693071 8.25 ug/L 96 46) Benzo (b) fluoranthene 33.16 252. 1142852 9.87 ug/L 93

{#) = qualifier out of range (m) = manual integration RFJ1404.D 5080402.M Fri Apr 05 06:38:59 2002 Page 1

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