GCMS reference results for sample AE06800, April 2002

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\040502\REFE0405.D Vial: 39 Acq On 7 Apr 2002 3:02 am Operator: Bohlk Sample REFl 3/22/02 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Apr 08 05:46:34 2002 Quant Results File: 5080402.RES

Quant Method C:\MSDCHEM\l\5973N\5080402.M (RTE Integrator) Title Quantitation For Method 508gcscan Last Update Fri Apr 05 05:56:22 2002 Response via Initial Calibration DataAcq Meth 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.46 152 850536 20.00 ug/L -0.01 10) Naphthalene-d8 12.93 136 3682447 20.00 ug/L -0.01 17). Acenaphthene-dl0 18.05 164 2126051 20.00 ug/L 0.00 29) Phenanthrene-dlO 22.41 188 3033139 20.00 ug/L -0.01 38) Chrysene-dl2 30.23 240 2391965 20.00 ug/L -0.02 44) Perylene-dl2 34.11 264 1516055 20.00 ug/L -0.01

System Monitoring Compounds 37) 2,4-DDD (SURR) 27.36 235 204538 6.79 ug/L 0.00 Spiked Amount 5.000 Recovery = 135.80%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 3.56 74 244919m 7.55 ug/L 3) bis(2-chloroethyl) ether 8.90 93 536661 11.35 ug/L 83 4) 1,3 - Dichlorobenze 9.29 146 392424 9.18 ug/L 95 5) 1,4 - Dichlorobenzene 9.50 146 404138 9.66 ug/L 95 6) 1,2 - Dichlorobenzene 9.88 146 361148 9.28 ug/L 98 7) 2,2 ' - oxybis (1-Chloropr 10.34 45 893321 12.24 ug/L. 93 8) N-Nitroso-di-n-propylamine 10.67 70 408870 11.36 ug/L . 94 9) Hexachloroethane 10.77 117 141009 8.78 ug/L 91 11) Nitrobenzene 11.02 77 475056 8.10 ug/L 98 12) Isophorone 11.73 82 1156460 10.93 ug/L 98 13) bis(2-Chloroethoxy) methan 12.47 93 687974 10.72 ug/L 98 14) 1,2,4-Trichlorobenzene 12.81 180 324009 10.17 ug/L 97 15) Naphthalene 12.99 128 1485874 11.69 ug/L 99 16) Hexachlorobutadiene 13.44 225 114332 7.25 ug/L 97 18) Hexachlorbcyclopentadiene 15.52 237 15122 1.32 ug/L 92 19) 2-chloronaphthalene 16.42 162 754558 10.29 ug/L 98 20) Dimethylphthalate 17.51 163 1077494 12.61 ug/L 99 21) 2,6-Dinitrotoluene 17.62 165 179209 9.92 ug/L 93 22) Acenaphthylene 17.60 152 1131498 11.23 ug/L 99 23) Acenaphthene 18.14 153 897183 12.57 ug/L 99 24) 2,4-Dinitrotoluene 18.77 165 196917 7.92 ug/L 91 25) Diethylphthalate 19.64 149 1065501 14.78 ug/L 98 26) 4-Chlorophenyl-phenyl ethe 19.81 204 475535 12.78 ug/L 99 27) Fluorene 19.67 166 1107249 13.62 ug/L 100 28) Azobenzen/ 1,2-Diphenylhyd 20.26 77 1492268 11.63 ug/L 93 30) N-Nitrosodiphenylamine 20.18 169 471949 8.86 ug/L 93 31) 4-Bromophenyl-phenyl ether 21.23 248 234560 12.94 ug/L 91 32) Hexachlorobenzene 21.26 284 222861 12.78 ug/L 80 33) Phenanthrene 22.47 178 1544880 13.81 ug/L 99 34) Anthracene 22.62 178 1335971 12.27 ug/L 97 35) Di-n-butylphthalate 24.57 149 1863526 14.72 ug/L 98 36) Fluoranthene 25.97 202 1518661 13.02 ug/L 82 39) Pyrene 26.60 202 1685424 12.06 ug/L 87 40) Butylbenzylphthalate 28,98 149 722164 11.92 ug/L 89 41) Benzo (a) antracene 30.21 228 1174291 12.26 ug/L 99 42) Bis (2-ethylhexyl) phthala 30.85 149 1068221 13.70 ug/L 97 43) Chrysene 30.29 228 1282128 13.97 ug/L 98 45) Di-n-Octylphthalate 32.70 149 1425323 9.81 ug/L 100 46) Benzo (b) fluoranthene 33.16 252 956423 11.67 ug/L 94

(#) = qualifier out of range (m) = manual integration REFE0405.D 5080402.M Mon Apr 08 O5':47:21 2002 Page 1

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