GCMS quantitative analysis results, sample AE06090, April 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File C:\MSDCHEM\1\DATA\ 0404 02B\C2 5JJ4 04.D Vial: 4 Acq On 5 Apr 2002 2:34 am Operator: Bohlk Sample C25 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Apr 05 06:19:31 2002 Quant Results File: 5080402.RES

Quant Method : C:\MSDCHEM\l\5973N\5080402.M (RTE Integrator) Title : Quantitation For Method 508gcscan Last Update : Fri Apr 05 05:56:22 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.47 152 1494924 20.00 ug/L 0.00 10) Naphthalene-d8 12.94 136 6234310 20.00 ug/L 0.00 17) Acenaphthene-dlO 18.06 164 3280180 20.00 ug/L 0.00 29) Phenanthrene-dlO 22.42 188 4893354 20.00 ug/L 0.00 38) Chrysene-dl2 30.25 240 3463773 20.00 ug/L 0.00 44) Perylene-dl2 34.11 264 1819919 20.00 ug/L 0.00

System Monitoring Compounds 37) 2,4-DDD (SURR) 27.35 235 28886 0.59 ug/L 0.00 Spiked Amount 5.000 Recovery = 11.80%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 3.48 74 1262323■ 22.13 ug/L 86 3) bis(2-chloroethyl) ether 8.91 93 1922531 23.14' ug/L 100 4) 1,3 - Dichlorobenze 9.30 146 1695819 22.56 ug/L 98 5) 1,4 - Dichlorobenzene 9.51 146 1695613 23.07 ug/L 96 6) 1,2 - Dichlorobenzene 9.89 146 1566571 22.91 ug/L 99 7) 2,2 ' - oxybis (1-Chloropr 10.35 45 2890240 22.53 ug/L 99 8) N-Nitroso-di-n-propylamine 10.70 70 1493879 23.61 ug/L 96 9) Hexachloroethane 10.77 117 688926 24.40 ug/L 94 11) Nitrobenzene 11.03 77 2207896 22.24 ug/L 98 12) Isophorone 11.75 82 3928235 21.92 ug/L 97 13) bis(2-Chloroethoxy) methan 12.49 93 2483649 22.86 ug/L 99 14) 1,2,4-Trichlorobenzene 12.82 180 1214792 22.52 ug/L 100 15) Naphthalene 13.00 128 4973195 23.11 ug/L 98 16) Hexachlorobutadiene 13.45 225 601013 22.51 ug/L 99 18) Hexachlorocyclopentadiene 15.52 237 381069 21.61 ug/L 99 19) 2-chloronaphthalene 16.43 162 2632144 23.26 ug/L 98 20) Dimethylphthalate 17.53 163 3056933 23.19 ug/L 100 21) 2,6-Dinitrotoluene 17.64 165 653576 23.45 ug/L 99 22) Acenaphthylene 17.61 152 3718834 23.91 ug/L 98 23) Acenaphthene 18.15 153 2564079 23.29 ug/L 99 24) 2,4-Dinitrotoluene 18.79 165 909121 23.70 ug/L 98 25) Diethylphthalate 19.68 149 2638946 23.73 ug/L 98 26) 4-Chlorophenyl-phenyl ethe 19.82 204 1322794 23.04 ug/L 98 27) Fluorene 19.68 166 2957587 23.58 ug/L 99 28) Azobenzen/ 1,2-Diphenylhyd 20.28 77 4553074 23.00 ug/L 94 30) N-Nitrosodiphenylamine 20.20 169 1966292 22.89 ug/L 100 31) 4-Bromophenyl-phenyl ether 21.24 248 661716 22.62 ug/L 91 32) Hexachlorobenzene 21.27 284 621485 22.08 ug/L 94 33) Phenanthrene 22.49 178 4072187 22.57 ug/L 99 34) Anthracene 22.63 178 4025597 22.93 ug/L 99 35) Di-n-butylphthalate 24.58 149 4796857 23.48 ug/L 99 36) Fluoranthene 25.98 202 4230515 22.48 ug/L 86 39) Pyrene 26.62 202 4423856 21.86 ug/L 89 40) Butylbenzylphthalate 28.98 149 2014755 22.97 ug/L 88 41) Benzo (a) antracene 30.21 228 3046928 21.97 ug/L 99 42) Bis (2-ethylhexyl) phthala 30.85 149 2653147 23.49 ug/L 98 43) Chrysene 30.31 228 2962495 22.29 ug/L 99 45) Di-n-Octylphthalate 32.70 149 4154524 23.82 ug/L 100 46) Benzo (b) fluoranthene 33.16 252 2192739 22.28 ug/L 94

(#) = qualifier out of range (m) = manual integration C25JJ404.D 5080402.M Fri Apr 05 06:20:07 2002 Page 1

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