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Document / 5 pages

GCMS method sheet for extraction parameters and logs, March 2002

Machine-extracted title · confidence 100%

Technical record detailing laboratory method parameters including drip rates, solvent lots, and extraction type logs.

NYC-WTC_000059661–000059665

Folder label: “GCMS X 3/13/02 A 3/27/02

Page image
Scanned page image, NYC-WTC_000059665
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

DFTPP

Data File C:\HPCHEM\1\DATA\MAR2102\DFTPP.D vial: 1 Acq On 21 Mar 2002 11:16 am Operator: Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE,Integrator) Title : 209 625/TCLP calibration table

Abundance TIC: DFTPP.D 3000000

2500000

2000000

1500000

1000000

500000

o' Time--> 25.00 25.20 25.40 25.60 25.80 26.00 26.20 26.40 26.60 26.80 27.00 27.20 27.40 27.60 27.80 28.00 28.20 28.40 28.60 Abundance Average of 26.828 (0 26.874 min.: DFTPP.D 200000 198

150000 442

100000 69 255 127 51 110 50000 275 224 ,1481 0 TT-p Jt- ............. 40 60 80_ 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 440

Spectrum Information: Average of 26.828 to 26.874 min.

Target Rei. to I Lower Upper Rei.' I Raw I Result Mass Mass I Limit% Limit% Abn% I Abn I Pass/Fail j

51 198 . 30 60 36.8 73285 PASS 68 69 0.00 2 0.0 0 PASS 69 198 0.00 100 48.2 95890 PASS 70 69 0.00 2 0.0 0 PASS 127 198 40 60 44.4 88294 PASS 197 198 0.00 1 0.0 0 PASS 198 198 100 100 100.0 199060 PASS 199 198 5 9 6.8 13438 PASS 275 198 10 30 22.9 45570 PASS 365 198 ' 1 100 2.4 4807 PASS 441 443 0.01 100 97.9 25718 PASS 442 198 40 110 68.0 135431 PASS 443 442 . 17 23 19.4 26279 PASS

DFTPP.D GCMS0308.M Mon Mar 25 08:42:52 2002

NYC-WTC_000059665

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NYC-WTC_000059665Source: NYC Law Department, mirrored locally

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