GCMS extraction log fragment with handwritten notes, Mar 2002

NYC 9/11 Public Portal Document

DFTPP

Data File : C:\HPCHEM\l\DATA\MAR2602\DFTPP.D Vial: 1 Acq On : 26 Mar 2002 8:44 am Operator: Sample : Inst : GC/MS 209 Mise : Multiplr: 1,00 MS Integration Params: GOOFY.P Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table

Abundance TIC: DFTPP.D ‘ 4000000-

3000000 I 2000000

1000000

Time^___ 04 A. izsoo 25!2O 25.40 25.60 25'80 26.00 26.20 26'40 26.60 26.80 27'oO 27.20 27.40 27.60 27.80 28.00 28.20 28.40 28.60 Abundance Average of 26.805 to 26.869 min.: DFTPP.D 198 200000 442

150000

. 69 127 255 i 100000 I 51 no 275 50000 224

m/z--> 0 40 60 ajUI I80 h?j111L. 24)2 1,^ 31 o3?3336 352365 333 403 423 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 440

Spectrum Information: Average of 26.805 to 26.869 min.

I Target Rei. to I Lower Upper Rei. Raw Result Mass Mass I Limit% Limit%' Abn% Abn Pass/Fail

51 198 30 60 35.3 78897 PASS 68 69 0.00 2 0.0 0 PASS 69 198 0.00 100 46.7 104438 PASS 70 69 0.00 2 0.0 0 PASS 1'27 198 40 60 42.9 95766 PASS 197 198 0.00 1 0.0 0 PASS 198 198 100 100 100.0 223469 PASS 199 198 5 9 6.8 15088 PASS 275 198 10 30 22.8 50955 PASS 365 198 1 100 2.4 5350 PASS 441 443 0.01 100 98.1 32294 PASS . 442 198 40 110 76.6 171182 PASS 443 442 17 23 19.2 32936 PASS

DFTPP.D GCMS0308.M Thu Mar 28 15:01:51 2002

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