GCMS document fragment with quality control data, March 2002

NYC 9/11 Public Portal Document

DFTPP

Data File C:\HPCHEM\1\DATA\MAR3 0 02\DFTPP.D Vial: 1 Acq On 29 Mar 2002 3:56 pm Operator: Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table

Abundance TIC: DFTPP.D i

3000000

■ 2000000

I , 1000000 !

O-i V Time-> 25'00 25'20 25.40 25.60 25^80 26'oo 25'20 26.40 26'60 26'80 27'oO 27.20 27.40 27.60 27.80 28.00 28.20 28.40 28.60 Abundance Average of 26.800 to 26.855 min.: DFTPP.D 198

200000 442

150000

69 127 255 ! 100000 51 110 275 50000 224 , 93 I I , ' 310'323336 352365 333 403 I 0 “H-r m/z-> 40 60 80 160 120 1^ 160 180 200 220 240 260 280 300 320 340 360 380 400 420 440

Spectrum Information: Average of 26.800 to 26.855 min.

I Target 1 Rei. to [ Lower | Upper 1 Rei. Raw I Result I Mass |. Mass j Limit% | Limit% | Abn% Abn I Pass/Fail

51 198 30 60 35.1 81740 PASS 68 69 0.00 2 0.0 0 PASS 69 198 0.00 100 45.8 106796 PASS 70 69 0.00 2 0.0 0 PASS . 127 198 40 60 42.7 99443 PASS 197 198 0.00 1 0.0 0 PASS 198 198 100 100 100.0 233078 PASS 199 198 5 9 6.6 15387 PASS 275 198 10 30 23.3 54213 PASS 365 198 1 100 2.4 / 5572 PASS 441 443 0.01 100 95.0 33127 PASS 442 198 40 110 77.6 180976 PASS 443 442 17 23 19.3 34857 PASS

DFTPP.D GCMS0308.M Tue Apr 02 12:26:25 2002

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