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GCMS method sheet for extraction parameters and logs, March 2002

Machine-extracted title · confidence 100%

Technical record detailing laboratory method parameters including drip rates, solvent lots, and extraction type logs.

NYC-WTC_000059661–000059665

Folder label: “GCMS X 3/13/02 A 3/27/02

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Scanned page image, NYC-WTC_000059664
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

DFTPP

Data File C:\HPCHEM\1\DATA\MAR2102\DFTPP2.D Vial: 1 Acq On 22 Mar 2002 8:58 am Operator: Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table

_____ 'Abundance

4000000 I , 3000000

2000000

1000000

0-^ I Time-->__ ^^00 25.20 25.40 25.60 25.8026 00 26.20 26.40 26.60 26.80 27.00 27.20 27.40 27,60 27,80 28.00 28.20 28.40 28.60 Abundance Average of 26.839 to 26.875 min.: DFTPP2.D 193

300000 442

200000 69 255 127 I 51 ; 100000 110 275 224

0 3P 1, j m/z--> 40 60 I80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 440

Spectrum information: Average of 26.839 to 26.875 min.

Target Rei. to Lower | Upper Rei. 1 Raw Result Mass Mass Limit% I Limit% j Abn% I Ahn Pass/Fail

51 198 30 60 34.9 125427 PASS 68 69 0.00 2 0.0 0 PASS 69 198 •0.00 100 46.4 166837 PASS 70 69 0.00 2 0.0 0 PASS 127 198 40 60 43.1 154816 PASS 197 198 0.00 1 0.0 0 PASS 198 198 100 100 100.0 359590 PASS 199 198 5 9 6.7 24043 PASS 275 198 10 30 23.3 / 83802 PASS 365 198 1 100 2.5 9030 PASS 441 443 0.01 100 99.2 51645 PASS 442 198 4 0. 110 75.3 270605 PASS 443 442 17 23 19.2 52046 PASS

DFTPP2.D GCMS0308.M Mon Mar 25 08:43:19 2002

NYC-WTC_000059664

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NYC-WTC_000059664Source: NYC Law Department, mirrored locally

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