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GCMS analysis results for sample AE05745, April 11 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE05745 conducted on April 11, 2002, including surrogate recovery data.

NYC-WTC_000059555–000059564

Folder label: “GCMS X 3/12/02 A 4/2/02

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Scanned page image, NYC-WTC_000059560
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NYC 9/11 Public Portal Document

LSC Area Percent Report

*' Data File C:\HPCHEM\1\DATA\APRO102\5746.D Vial: 25 Acq On 3 Apr 2002 12:59 am Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0403.M (RTE Integrator)' Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.136 332 337 350 rBV 95953 270213 6.56% 1.451% 2 8.282 350 353 361 rVB 16983 41514 1.01% 0.223% 3 12.248 779 785 799 rVB 1132630 2790083 67.78% 14.984% 4 15.884 1175, 1181 1195 rBV 1786514 3632343 88.24% 19.507% 5 21.190 1752 1759 1777 rBV 2037331 4116602 100.00% 22.108%

6 25.633 2236 2243 2254 rBV2 1854327 3824087 92.89% 20.537% 7 30.710 2790 2796 2801 rBV 198940 408436 9.92% 2.193% 8 33.694 3114 3121 3137 rBV2 923862 2153879 52.32% 11.567% 9 37.935 3575 3583 3596 rBV2 463015 1383421 33.61% 7.430%

Sum of corrected areas: 18620578

5746.D GCMS0403.M Fri Apr 05 10:38:22 2002

NYC-WTC_000059560

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NYC-WTC_000059560Source: NYC Law Department, mirrored locally

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