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GCMS calibration results for sample AE03076, March 2002

Machine-extracted title · confidence 100%

Laboratory report showing GC/MS calibration data and surrogate recovery for sample AE03076 on March 22, 2002.

NYC-WTC_000011105–000011112

Folder label: “GCMS X 2/12/02 A 3/19/02

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Scanned page image, NYC-WTC_000011108
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

‘ ‘Data File C:\HPCHEM\1\DATA\MAR0102\3076.D Vial: 28 Acq On 2 Mar 2002 12:51 pm Operator: Sample gc/ms scan 2/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 8.197 339 344 351 rBV 27521 69214 2.11% 0.420% 2 12.319 787 793 813 rVB 877201 2249319 68.62% 13.648% 3 15.955 1183 1189 1207 rBV 1344518 3029214 92.41% 18.380% 4 21.270 1761 1768 1788 rBV 1495953 3278073 100.00% 19.890% 5 25.723 2245 2253 2264 rBV2 1333460 3167173 96.62% 19.218%

6 25.851 2264 2267 2279 rVB 13565 42729 1.30% 0.259% 7 30.790 2800 2805 2818 rVB 152198 314246 9.59% 1.907% 8 33.783 3124 3131 3151 rBV2 1026374 2456430 74.94% 14.905% 9 38.061 3588 3597 3616 rBV2 579320 1874259 57.18% 11.372%

Sum of corrected areas: 16480657

3076.D GCMS0208.M Tue Mar 05 14:45:28 2002

NYC-WTC_000011108

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NYC-WTC_000011108Source: NYC Law Department, mirrored locally

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