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GCMS analysis results for sample AE02599, Mar 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE02599 conducted on March 7, 2002, including surrogate recovery data.

NYC-WTC_000005302–000005311

Folder label: “GCMS X 2/5/02 A 3/1/02

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Scanned page image, NYC-WTC_000005307
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document LSC Area Percent Report

. Data File C:\HPCHEM\1\DATA\MAR0102\2599.D Vial: 9 Acq On 1 Mar 2002 4:14 pm Operator: Sample gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.195 339 343 351 rBV 10569 27145 1.20% 0.235% 2 12.317 786 792 808 rVB 640701 1562037 69.26% 13.541% 3 15.953 1182 1188 1206 rBV 928790 2080872 92.27% 18.038% 4 21.268 1761 1767 1783 rBV 1049022 2255215 100.00% 19.550% 5 25.711 2245 2251 2263 rBV2 922161 2158147 95.70% 18.708%

6 25.849 2263 2266 2273 rVB2 8719 25017 1.11% 0.217% 7 30.797 2799 2805 2813 rVB 134078 284394 12.61% 2.465% 8 33.781 3123 3130 3146 rBV2 747815 1742462 77.26% 15.105% 9 38.059 3587 3596 3612 rBV2 436547 1400465 62.10% 12.140%

Sum of corrected areas: 11535754

2599.D GCMS0208.M Mon Mar 04 11:43:15 2002

NYC-WTC_000005307

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NYC-WTC_000005307Source: NYC Law Department, mirrored locally

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