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GCMS analysis results for sample AE02602, Mar 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE02602 conducted on March 7, 2002, including surrogate recovery data.

NYC-WTC_000005322–000005332

Folder label: “GCMS X 2/5/02 A 3/1/02

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Scanned page image, NYC-WTC_000005327
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NYC 9/11 Public Portal Document LSC Area Percent Report

. Data File C:\HPCHEM\l\DATA\MAR0102\2602.D Vial: 12 Acq On 1 Mar 2002 7:11 pm Operator: Sample gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.198 340 344 351 rBV 11645 28203 1.23% 0.244% 2 12.311 787 792 807 rVB 618731 1571702 68.46% 13.575% 3 15.955 1183 1189 1207 rBV 960535 2116739 92.20% 18.283% 4 21.271 1761 1768 1780 rBV 1045168 2295828 100.00% 19.829% 5 25.714 2245 2252 2264 rBV2 957766 2191295 95.45% 18.927%

6 25.852 2264 2267 2274 rVB 9698 24816 1.08% 0.214% 7 30.791 2800 2805 2812 rBV 152287 306613 13.36% 2.648% 8 33.490 3090 3099 3111 rBV3 8132 33743 1.47% 0.291% 9 33.783 3124 3131 3150 rBV2 702079 1690167 73.62% 14.598% 10 38.052 3587 3596 3616 rBV 418397 _ 1318799 57.44% 11.391%

Sum of corrected areas: 11577905

2602.D GCMS0208.M Mon Mar 04 11:46:05 2002

NYC-WTC_000005327

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NYC-WTC_000005327Source: NYC Law Department, mirrored locally

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