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GCMS analysis results for sample AE05702, April 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE05702 conducted on April 11, 2002, including surrogate recovery data.

NYC-WTC_000059517–000059525

Folder label: “GCMS X 3/12/02 A 4/2/02

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Scanned page image, NYC-WTC_000059522
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

■’ Data File C:\HPCHEM\l\DATA\APR0102\5703.D Vial: 21 Acq On 2 Apr 2002 8:04 am Operator: Sample gc/ms scan 3/12 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0403.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5-

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.127 332 336 350 rBV 94702 260140 6.35% 1.376% 2 12.249 779 785 803 rVB 1175850 2821012 68.90% 14.923% 3 15.885 1175 1181 1198 rBV 1752279 3631729 88.70% 19.212% 4 21.191 1752 1759 1774 rBV 1972317 4094405 100.00% 21.659% 5 25.634 2236 2243 2255 rBV2 1806377 3801231 92.84% 20.108%

6 30.711 2791 2796 2803 rBV 208170 403067 9.84% 2.132% 7 33.694 3114 3121 3137 rBV 1049575 2331949 56.95% 12.336% 8 37.936 3575 3583 3597 rBV2 521156 1560156 38.10% 8.253%

Sum of corrected areas: 18903689

5703.D GCMS0403.M Fri Apr 05 10:35:22 2002

NYC-WTC_000059522

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NYC-WTC_000059522Source: NYC Law Department, mirrored locally

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