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GCMS analysis results for sample AE05701, April 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE05701 conducted on April 11, 2002, including surrogate recovery data.

NYC-WTC_000059508–000059516

Folder label: “GCMS X 3/12/02 A 4/2/02

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Scanned page image, NYC-WTC_000059513
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NYC 9/11 Public Portal Document

LSC Area Percent Report

• Data File C:\HPCHEM\l\DATA\APR0102\5702.D Vial: 20 Acq On 2 Apr 2002 7:05 am Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0403.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.128 332 336 354 rBV 106202 289357 6.17% 1.356% 2 12.250 779 785 801 rVB 1291954 3169367 67.54% 14.857% 3 15.885 1175 1181 1197 rBV 2004415 4102551 87.43% 19.231% 4 21.191 1752 1759 1774 rBV 2288797 4692630 100.00% 21.998% 5 25.635 2236 2243 2254 .rBV2 2002758 4311426 91.'88%. 20.211%

6 30.711 2790 2796 2805 rVB 224955 448009 9.55% 2.100% 7 33.695 3114 3121 3141 rBV2 1123852 2570644 54.78% 12.050% 8 37.936 3575 3583 3603 rBV2 565830 1748568 37.26% 8.197%

Sum of corrected areas: 21332552

5702.D GCMS0403.M Fri Apr 05 10:34:46 2002

NYC-WTC_000059513

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NYC-WTC_000059513Source: NYC Law Department, mirrored locally

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