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GCMS reference analysis results for sample AE05701, April 2002

Machine-extracted title · confidence 90%

Reference analysis report for sample AE05701 conducted on April 5, 2002, quantifying recovery of specific organic compounds.

NYC-WTC_000059499–000059507

Folder label: “GCMS X 3/12/02 A 4/2/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\APR0102\5701.D Vial: 19 Acq On 2 Apr 2002 6:05 am Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0403.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.133 332 336 343 rBV 106332 235404 5.13% 1.134% 2 12.246 779 784 801 rVB 1319113 3123930 68.06% 15.043% 3 15.881 1174 1180 1197 rBV 1911305 4050232 88.24% 19.504% 4 21.188 1752 1758 1772 rBV 2127655 4589832 100.00% 22.103% 5 25.631 2236 2242 2254 rBV2 1893841 4248152 92.56% 20.457%

6 30.708 2788 2795 2806 rVB 212777 416906 9.08% 2.008% 7 33.691 3114 3120 3136 rBV2 1071665 2462585 53.65% 11.859% 8 37.942 3574 3583 3598 rBV2 538077 1639049 35.71% 7.893%

Sum of corrected areas: 20766090

5701.D GCMS0403.M Fri Apr 05 10:34:09 2002

NYC-WTC_000059504

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NYC-WTC_000059504Source: NYC Law Department, mirrored locally

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